Aluyi H A, Drucker D B
J Chromatogr. 1979 Oct 19;178(1):209-18. doi: 10.1016/s0021-9673(00)89709-5.
A modified method is described for the analysis, by gas-liquid chromatography, of various sugars as the trimethylsilyl derivatives of their methyl glycosides. The technique was employed for the analysis of the cellular carbohydrate of Streptococcus mutans NCTC 10832 and provided reproducible fingerprints, consisting of peaks due to glycerol, rhamnose, xylose, galactofuranse, glucose, N-acetylglucosamine and N-acetylmuramic acid. Absolute identification of the latter was by combined gas-liquid chromatography--mass spectrometry.
本文描述了一种改进的方法，用于通过气液色谱法分析各种糖类，将其作为甲基糖苷的三甲基硅烷基衍生物。该技术用于分析变形链球菌NCTC 10832的细胞碳水化合物，并提供了可重复的指纹图谱，其中包括甘油、鼠李糖、木糖、呋喃半乳糖、葡萄糖、N-乙酰葡糖胺和N-乙酰胞壁酸产生的峰。后者的绝对鉴定采用气液色谱-质谱联用。
