肌毒素四乙酸酯的核磁共振和质谱研究
Nuclear-magnetic-resonance and mass-spectral study of myxinol tetra-acetate.
作者信息
Cross A D
出版信息
Biochem J. 1966 Jul;100(1):238-41. doi: 10.1042/bj1000238.
Abstract
Myxinol tetra-acetate was examined by both nuclear-magnetic-resonance and mass-spectral techniques. The results are compared with corresponding data for 5alpha-ranol tetra-acetate and 5alpha-cyprinol tetra-acetate. The structure deduced for myxinol tetra-acetate, 3beta,7alpha,16alpha,27-tetrahydroxy-5beta-cholestane, is in agreement with that simultaneously arrived at by Haslewood (1966).
摘要
采用核磁共振和质谱技术对岩鱼醇四乙酸酯进行了检测。并将结果与5α-鲨肝醇四乙酸酯和5α-鲤醇四乙酸酯的相应数据进行了比较。推断出的岩鱼醇四乙酸酯结构为3β,7α,16α,27-四羟基-5β-胆甾烷，这与哈斯勒伍德（1966年）同时得出的结构一致。
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引用本文的文献
1
New evidence for the structure of myxinol.肌醇结构的新证据。
Biochem J. 1967 Sep;104(3):1061-3. doi: 10.1042/bj1041061.
2
Comparative studies of bile salts. 16-Deoxymyxinol, a second bile alcohol from hagfish.胆汁盐的比较研究。16-脱氧粘醇，一种来自盲鳗的第二种胆汁醇。
Biochem J. 1969 May;112(5):763-5. doi: 10.1042/bj1120763.
本文引用的文献
1
STEROIDS. CCLXXVII. SPECTRA AND STEREOCHEMISTRY. XIX. A COMPARATIVE STUDY OF THE NMR SPECTRA OF SOME STEROIDS IN FIVE SOLVENTS. THE STRUCTURE OF 'ACIPENSEROL-A'.
Steroids. 1965 May;6:655-62. doi: 10.1016/0039-128x(65)90158-3.
2
Comparative studies of bile salts, myxinol disulphate, the principal bile salt of hagfish (Myxinidae).对胆汁盐、硫酸黏液醇（盲鳗科主要胆汁盐）的比较研究。
Biochem J. 1966 Jul;100(1):233-7. doi: 10.1042/bj1000233.
3
Nuclear-magnetic-resonance and mass-spectral analysis of ranol tetra-acetate.雷诺四乙酸酯的核磁共振与质谱分析
Biochem J. 1964 Feb;90(2):314-5. doi: 10.1042/bj0900314.
4
A nuclear magnetic resonance spectral study of cyprinol.鲤醇的核磁共振光谱研究。
Biochem J. 1964 Feb;90(2):308-9. doi: 10.1042/bj0900308.
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