一种用于分析鸡血中玉米赤霉烯酮的高压液相色谱法。
A high pressure liquid chromatographic method for the analysis of zearalenone in chicken blood.
作者信息
Turner G V, Phillips T D, Heidelbaugh N D, Russell L H
出版信息
J Environ Sci Health B. 1982;17(4):297-309. doi: 10.1080/03601238209372322.
A high pressure liquid chromatographic (HPLC) method is described to determine zearalenone in chicken blood. Samples are extracted with acetonitrile, followed by a hexane cleanup procedure and extracted further with ethyl acetate. The analysis of zearalenone is by HPLC using a reverse phase radial compression separation system, an ultraviolet absorbance detector and a mobile phase of acetonitrile-water 60:40 (v/v). Recoveries of zearalenone in blood at levels of 50-200 ng/ml are in the range of 66.8-72.6%.
描述了一种用于测定鸡血中玉米赤霉烯酮的高压液相色谱（HPLC）方法。样品先用乙腈提取，接着进行己烷净化程序，然后再用乙酸乙酯进一步提取。玉米赤霉烯酮的分析采用HPLC，使用反相径向压缩分离系统、紫外吸收检测器以及乙腈 - 水（60:40，v/v）的流动相。血样中浓度为50 - 200 ng/ml的玉米赤霉烯酮回收率在66.8% - 72.6%范围内。
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