Kossoy A D, Cooke G C
J Pharm Sci. 1978 May;67(5):722-5. doi: 10.1002/jps.2600670547.
An investigation of the products resulting from the photolysis of apridine hydrochloride is described. The compounds were characterized by GLC spiking experiments and combined GLC--mass spectrometry. In some cases, Rf values derived from TLC and/or preparative TLC and subsequent high-resolution mass spectral measurements also were employed for identification.
本文描述了对盐酸阿普立定光解产物的研究。这些化合物通过气相色谱(GLC)加样实验和气相色谱-质谱联用进行表征。在某些情况下,还采用了薄层色谱(TLC)和/或制备型TLC得到的比移值(Rf)以及随后的高分辨率质谱测量来进行鉴定。