Rhea U S, Gilchrist J E, Peeler J T, Shah D B
J Assoc Off Anal Chem. 1984 Sep-Oct;67(5):942-5.
Two can leak tests were compared by 7 collaborators. In the helium leak test, pressurized helium is applied to the outside of the container, and a headspace gas sample from the can is then analyzed for the presence of helium. The vacuum test is described in the Bacteriological Analytical Manual. Ninety No. 303 cans of creamed-style corn, green beans, carrots, fruit cocktail, and whole-kernel corn were shipped in 3 groups. Two groups of 30 cans had 10 dented flat cans, 5 flat controls (nondented), 10 dented swollen cans, and 5 swollen control cans (nondented). The third group had 10 dented swollen cans and 5 swollen control cans. Of 600 cans analyzed, 37 (6.2%) were deleted from the analysis because results were not available for both tests. One laboratory was constrained by scheduling to analyze 15 of 45 swollen cans. The helium leak test found 12 (13%) positives of 92 nondented swollen cans. One pressurization test yielded 7 of those 12 positives. Of the 400 dented cans sent as possible leakers, the helium test found 267 positives, and the vacuum test found 181. Five of the 7 analysts had significantly (alpha = 0.05) higher percent positive helium results. One analyst found more leakers by the vacuum leak test. Both tests found fewer positives in the swollen dented cans than in the flat dented cans. After exposure to pressurized helium, all cans with greater than 8 psi headspace pressure were positive helium leakers. The method was adopted official first action.
7位合作者对两种泄漏测试方法进行了比较。在氦气泄漏测试中,将加压氦气施加到容器外部,然后分析罐顶空气样本中是否存在氦气。真空测试在《细菌学分析手册》中有描述。90罐303号罐装奶油玉米、青豆、胡萝卜、什锦水果罐头和整粒玉米被分成3组运送。两组各30罐,其中有10罐凹瘪扁平罐、5个扁平对照罐(无凹痕)、10罐凹瘪膨胀罐和5个膨胀对照罐(无凹痕)。第三组有10罐凹瘪膨胀罐和5个膨胀对照罐。在分析的600罐中,有37罐(6.2%)因两种测试结果均不可用而从分析中剔除。一个实验室由于时间安排限制,只分析了45个膨胀罐中的15个。氦气泄漏测试在92个无凹痕膨胀罐中发现了12个(13%)阳性结果。其中12个阳性结果中有7个来自一次加压测试。在作为可能泄漏罐送去检测的400个凹瘪罐中,氦气测试发现267个阳性,真空测试发现181个阳性。7位分析人员中有5位的氦气阳性结果百分比显著更高(α = 0.05)。有一位分析人员通过真空泄漏测试发现了更多的泄漏罐。两种测试在凹瘪膨胀罐中发现的阳性结果都比在扁平凹瘪罐中少。在暴露于加压氦气后,所有顶空压力大于8 psi的罐都是氦气阳性泄漏罐。该方法首次被官方采用。