Shotwell O L, Hesseltine C W
J Assoc Off Anal Chem. 1983 Nov;66(6):1466-9.
Every year during the 5-year period 1976-1980, approximately 100 samples each of corn and wheat from trucks delivering the grains at elevators in Virginia were collected by personnel of the Federal Grain Inspection Service and shipped to NRRC. Samples were analyzed as soon as possible for aflatoxin, zearalenone, and ochratoxin A. The 3 mycotoxins were not detected in any wheat sample. Zearalenone and ochratoxin A were not found in any corn sample; however, aflatoxin was detected in at least 25% of the corn samples from every crop year. In 1976-1980, the incidence of aflatoxin at levels of 20 ng/g or more (the Food and Drug Administration guideline) ranged from 18 to 61%; aflatoxin incidence above 100 ng/g was 5-29%. The average aflatoxin levels in corn samples collected in the 5 years varied from 21 to 137 ng/g. Moisture content of the samples was not determined, so aflatoxin levels given may be higher than they were at harvest. However, there are obviously differences from year to year. In freshly harvested corn samples collected by fieldmen of the Statistical Reporting Service in yield surveys in 1978 and 1979, aflatoxin incidence above the FDA guideline was 10 and 13%, and above 100 ng/g was 4 and 7%. The average aflatoxin level in all samples collected in 1978 was 13 ng/g and in 1979, 36 ng/g. Some aflatoxin can be expected yearly in Virginia corn, but the incidence and levels vary from year to year.
在1976年至1980年这5年期间,每年联邦谷物检验局的工作人员会从弗吉尼亚州谷物升降机处运送谷物的卡车上收集约100份玉米和小麦样本,并运往国家研究资源中心(NRRC)。样本会尽快进行黄曲霉毒素、玉米赤霉烯酮和赭曲霉毒素A的分析。在任何小麦样本中均未检测到这3种霉菌毒素。在任何玉米样本中均未发现玉米赤霉烯酮和赭曲霉毒素A;然而,在每个作物年度至少25%的玉米样本中检测到了黄曲霉毒素。1976年至1980年,黄曲霉毒素含量达到20纳克/克或更高(食品药品监督管理局的指导标准)的发生率在18%至61%之间;黄曲霉毒素含量高于100纳克/克的发生率为5%至29%。这5年收集的玉米样本中黄曲霉毒素的平均含量在21至137纳克/克之间。未测定样本的水分含量,因此给出的黄曲霉毒素含量可能高于收获时的含量。然而,年份之间显然存在差异。在1978年和1979年产量调查中由统计报告服务处的外勤人员收集的新鲜收获玉米样本中,高于食品药品监督管理局指导标准的黄曲霉毒素发生率分别为10%和13%,高于100纳克/克的发生率分别为4%和7%。1978年收集的所有样本中黄曲霉毒素的平均含量为13纳克/克,1979年为36纳克/克。预计弗吉尼亚州的玉米每年都会有一定量的黄曲霉毒素,但发生率和含量会因年份而异。