Spiegel H E, Opar G E
J Chromatogr. 1978 Aug 1;155(1):159-67. doi: 10.1016/s0021-9673(00)83945-x.
A simple and easily manipulated method is described for th- determination of total urinary phenol. This modification of earlier procedures incorporates the enzymatic hydrolysis of conjugated phenol, extraction of the hydrolysis products into isopropyl ether and final quantitation by gas-liquid chromatography-flame ionization detection. The method employs benzyl alcohol as internal standard.
本文描述了一种用于测定尿中总酚的简单且易于操作的方法。这种对早期方法的改进包括对结合酚进行酶促水解,将水解产物萃取到异丙醚中,并最终通过气液色谱 - 火焰离子化检测进行定量。该方法使用苯甲醇作为内标。