• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利:CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验

乌洛托品的电导测定法。

Conductometric determination of methenamine.

作者信息

Nikolić K I, Velasević K R, Arsenijević L S

出版信息

Pharm Weekbl Sci. 1983 Feb 25;5(1):28-30. doi: 10.1007/BF01959648.

DOI:10.1007/BF01959648
PMID:6844123
Abstract

A method of conductometric titration for determination of methenamine is presented. An aqueous solution of silicotungstic acid is used as titrant. The acid and methenamine form an insoluble compound in which the molar ratio of the acid to methenamine is 1:4. Conductometric curves were obtained, the shapes of which are suitable for accurate and reproducible determination of the end point of titration. The results show reasonable accuracy. Good reproducibility was achieved even when small quantities of methenamine had to be determined.

摘要

提出了一种用于测定乌洛托品的电导滴定法。使用硅钨酸水溶液作为滴定剂。该酸与乌洛托品形成一种不溶性化合物,其中酸与乌洛托品的摩尔比为1:4。获得了电导曲线,其形状适用于准确且可重复地测定滴定终点。结果显示出合理的准确度。即使在必须测定少量乌洛托品时也实现了良好的重现性。

相似文献

1
Conductometric determination of methenamine.乌洛托品的电导测定法。
Pharm Weekbl Sci. 1983 Feb 25;5(1):28-30. doi: 10.1007/BF01959648.
2
Spectrophotometric determination of methenamine and its salts by 2-hydrazinobenzothiazole.用2-肼基苯并噻唑分光光度法测定乌洛托品及其盐类。
J Pharm Sci. 1973 Sep;62(9):1503-4. doi: 10.1002/jps.2600620926.
3
[Complexometric titration in pharmaceutical analysis. XI. Indirect determination of hexamethylenetetramine and isonicotinic acid hydrazide].[药物分析中的络合滴定法。XI. 乌洛托品和异烟肼的间接测定]
Cesk Farm. 1955 May;4(4):185-6.
4
[Analysis of ternary solutions by means of measuring of the refraction index and determination of total molal or gram-equivalent content of 2 components].通过测量折射率和测定两种组分的总摩尔含量或克当量含量来分析三元溶液
Farmatsiia. 1969 Jul-Aug;18(4):55-9.
5
[Acid-base titrations in an alcoholic medium. IV. Conductometric titration curves].
Pharm Weekbl. 1965 Dec 24;100(52):1526-49.
6
GLC determination of methenamine in tablets.片剂中乌洛托品的葡萄糖酸氯己定测定法。 (注:这里原文表述似乎有误,推测正确的应该是“Glucose determination of methenamine in tablets”,即“片剂中乌洛托品的葡萄糖测定法” ,以上是按纠正后内容翻译的,如果按照原错误内容严格翻译是“片剂中乌洛托品的葡萄糖酸氯己定测定” ,这样不太符合正常逻辑,所以建议确认下原文)
J Pharm Sci. 1977 Apr;66(4):589-90. doi: 10.1002/jps.2600660435.
7
Conductometric method for the quantitative analysis of Pb(II) and Cd(II) with 2-mercapto-5-R-amino-1, 3, 4-thiadiazole derivatives.用2-巯基-5-R-氨基-1,3,4-噻二唑衍生物对铅(II)和镉(II)进行定量分析的电导法
J Pharm Biomed Anal. 1998 Oct;18(1-2):83-91. doi: 10.1016/s0731-7085(98)00152-6.
8
Transport properties and association behaviour of the zwitterionic drug 5-aminolevulinic acid in water. A precision conductometric study.
Eur J Pharm Sci. 2004 Feb;21(2-3):347-50. doi: 10.1016/j.ejps.2003.10.027.
9
[Conductometric analysis in the manufacturing and control of chemico-pharmaceutic preparations. 3. Conductometric titration and some physico-chemical characteristics of apressin].
Med Prom SSSR. 1965 Sep;19(9):57-9.
10
Determination of methenamine, methenamine mandelate and methenamine hippurate in pharmaceutical preparations using ion-exchange HPLC.采用离子交换高效液相色谱法测定药物制剂中的乌洛托品、乌洛托品扁桃酸盐和乌洛托品马尿酸盐。
J Pharm Biomed Anal. 2006 Mar 18;40(5):1243-8. doi: 10.1016/j.jpba.2005.09.017. Epub 2005 Nov 17.

本文引用的文献

1
[Polarometric titration of nitrogen-containing organic bases with the aid of heteropolyacid and nitro compounds].
Pharmazie. 1955 Mar;10(3):170-80.