Kawada E
Shika Rikogaku Zasshi. 1980 Apr;21(54):150-62.
In this study, the author attempted to find out the suitable methods of surface treatments for non-precious metal-ceramics alloys. Three Ni-Cr system alloys in the market, (Gemini II, Euro-ceram and Wiron S) were used. The shear bond strength was measured under the various conditions, varying the heating temperatures of pre-oxidation treatment and finishing methods of the metal surface. A specially designed apparatus which had been improved by the author, was used to measure the shear bod strength of the metal-ceramics. The following results were obtained. 1. The testing method improved was found better as a means of measuring the bond strength. Because the shear bond strength which was obtained by this testing method was hardly affected by the compressive force originating from porcelain contraction or the strength of alloys. 2. In the case of Gemini II and Euro-ceram, the influence of the finishing treatment on the properties was great. The coarser the surface roughness, the greater the value of the shear bond strength. 3. In the case of Wiron S, the influence of the pre-oxidation treatment was great. The higher the temperature of treatment, the greater the value of shear bond strength. 4. The optimum surface treatment of metal was obtained among three alloys respectively. The shear bond strength of Gemini II was greater than the others under any condition. In the case of Euro-ceram, the highest bond strength was obtained under the coarser surface condition regardless of the temperature of pre-oxidation treatment. In the case of Wiron S, the highest bond strength was obtained by the surface which was finished by the #600 emerypaper and the higher temperature of pre-oxidation treatment.
在本研究中,作者试图找出非贵金属烤瓷合金合适的表面处理方法。使用了市场上三种镍铬系合金(Gemini II、Euro-ceram和Wiron S)。在不同条件下测量剪切粘结强度,改变预氧化处理的加热温度和金属表面的精加工方法。使用作者改进的专门设计的仪器来测量金属烤瓷的剪切粘结强度。得到了以下结果。1. 改进后的测试方法作为测量粘结强度的手段更好。因为通过这种测试方法获得的剪切粘结强度几乎不受瓷收缩产生的压缩力或合金强度的影响。2. 对于Gemini II和Euro-ceram,精加工处理对性能的影响很大。表面粗糙度越粗,剪切粘结强度值越大。3. 对于Wiron S,预氧化处理的影响很大。处理温度越高,剪切粘结强度值越大。4. 分别在三种合金中获得了金属的最佳表面处理。在任何条件下,Gemini II的剪切粘结强度都大于其他合金。对于Euro-ceram,无论预氧化处理温度如何,在较粗的表面条件下都能获得最高的粘结强度。对于Wiron S,通过用#600砂纸精加工且预氧化处理温度较高的表面能获得最高的粘结强度。