Kitada Y, Sasaki M, Tanigawa K
J Assoc Off Anal Chem. 1982 Nov;65(6):1302-4.
A simple, rapid, efficient method has been developed for determining thiabendazole, o-phenylphenol, and diphenyl in citrus fruits by using high performance liquid chromatography, with fluorescence or ultraviolet detection. The compounds are extracted with ethyl acetate and separated from soluble fruit components on a LiChrosorb RP-8 column. Recovery of these compounds added to citrus fruits at 5 or 50 ppm levels was greater than 93%; the limit of detection for the compounds is 1 ppm.
已开发出一种简单、快速、高效的方法，通过使用配备荧光或紫外检测的高效液相色谱法来测定柑橘类水果中的噻苯达唑、邻苯基苯酚和联苯。这些化合物用乙酸乙酯萃取，并在LiChrosorb RP - 8柱上与水果中的可溶性成分分离。添加到柑橘类水果中浓度为5或50 ppm的这些化合物的回收率大于93%；这些化合物的检测限为1 ppm。
