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血液中铅的原子吸收测定法的改进。

Improvement in the atomic absorption determination of lead in blood.

作者信息

Karai I, Fukumoto K, Horiguchi S

出版信息

J Appl Toxicol. 1981 Dec;1(6):295-6. doi: 10.1002/jat.2550010604.

DOI:10.1002/jat.2550010604
PMID:7185890
Abstract

A simple, precise and accurate analysis for lead in blood and tissue was developed using spectrophotometry after extraction with HCl, H3PO4, KI and methyl isobutyl ketone. The results were similar to those obtained by anodic stripping voltammetry. The method is simple, requires only four reagents, does not need pH adjustment for lead extraction, saves time and is suitable for analyzing a large number of specimens.

摘要

采用盐酸、磷酸、碘化钾和甲基异丁基酮萃取后用分光光度法建立了一种简单、精确且准确的血液和组织中铅的分析方法。结果与阳极溶出伏安法获得的结果相似。该方法简单,仅需四种试剂,铅萃取无需调节pH值,节省时间,适用于大量样本的分析。

相似文献

1
Improvement in the atomic absorption determination of lead in blood.血液中铅的原子吸收测定法的改进。
J Appl Toxicol. 1981 Dec;1(6):295-6. doi: 10.1002/jat.2550010604.
2
[Comparison between anodic stripping voltammetry and graphite furnace atomic absorption spectrophotometry for blood lead analysis].阳极溶出伏安法与石墨炉原子吸收分光光度法用于血铅分析的比较
Wei Sheng Yan Jiu. 2007 Jan;36(1):90-2.
3
Anodic stripping voltammetry compared with graphite furnace atomic absorption spectrophotometry for blood lead analysis.阳极溶出伏安法与石墨炉原子吸收分光光度法用于血铅分析的比较
Clin Chem. 2001 Sep;47(9):1703-4.
4
Direct methods for the determination of lead in whole blood by anodic stripping voltammetry.
Am J Med Technol. 1980 Dec;46(12):853-7.
5
A comparison of two methods for the determination of thallium in urine. Differential pulse anodic stripping voltammetry and flameless atomic absorption spectrophotometry.
Ann Clin Biochem. 1983 Sep;20 (Pt 5):321-6. doi: 10.1177/000456328302000514.
6
Rapid micromethod for blood lead analysis by anodic stripping voltammetry.阳极溶出伏安法快速微量血铅分析法
Clin Chem. 1976 Feb;22(2):221-3.
7
[Microdetermination of lead and cadmium in blood and urine by graphite furnace atomic absorption spectrophotometry (author's transl)].石墨炉原子吸收分光光度法微量测定血液和尿液中的铅和镉(作者译)
Clin Chim Acta. 1979 Jan 1;91(1):41-6. doi: 10.1016/0009-8981(79)90468-6.
8
[Blood lead analysis by wet ashing, solvent extraction and flameless atomic absorption spectrophotometry (author's transl)].
Med Lav. 1979 Jul-Aug;70(4):313-7.
9
[Studies on the direct extraction method for determination of lead in blood by atomic absorption spectrophotometry (author's transl)].
Rinsho Byori. 1978 Jul;26(7):611-4.
10
Lead in preserved duck eggs: field screening test and confirmation and quantitation by atomic absorption spectrophotometry and anodic stripping voltammetry.松花蛋中的铅:现场筛选试验以及采用原子吸收分光光度法和阳极溶出伏安法进行确认和定量分析。
J Assoc Off Anal Chem. 1981 Jul;64(4):1014-6.

引用本文的文献

1
Erythrocyte arginase activity as an indicator of lead exposure.红细胞精氨酸酶活性作为铅暴露的指标。
Br J Ind Med. 1983 Feb;40(1):106-10. doi: 10.1136/oem.40.1.106.