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通过中子活化快速测定生物体液中的总溴和碘。

The rapid determination of total bromine and iodine in biological fluids by neutron activation.

作者信息

Holzbecher J, Ryan D E

出版信息

Clin Biochem. 1980 Dec;13(6):277-8. doi: 10.1016/s0009-9120(80)80009-9.

DOI:10.1016/s0009-9120(80)80009-9
PMID:7214696
Abstract

Total bromine and iodine are instrumentally determined in 1 mL samples of body fluids by neutron activation under a boron shield at normal concentration levels. No sample treatment is necessary. Bromine is determined by its 80Br nuclide (617.0 keV; T1/2 = 18.0 min) and iodine by its 128I nuclide (442.7 keV;T1/2 = 25.0 min). The method is rapid; four bromine and two iodine determinations can be done in one hour. Bromine and iodine can be detected down to 14 micrograms/dL (1.75 mumol/L) and 2.9 micrograms/dL (0.23 mumol/L), respectively.

摘要

在硼屏蔽下,通过中子活化法对1毫升体液样本中的总溴和碘进行仪器测定,适用于正常浓度水平。无需对样本进行处理。溴通过其80Br核素(617.0 keV;半衰期=18.0分钟)测定,碘通过其128I核素(442.7 keV;半衰期=25.0分钟)测定。该方法快速;一小时内可进行四次溴和两次碘的测定。溴和碘的检测下限分别可达14微克/分升(1.75微摩尔/升)和2.9微克/分升(0.23微摩尔/升)。

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