Miceli J N, Bowman D B, Aravind M K
J Anal Toxicol. 1981 Jan-Feb;5(1):29-32. doi: 10.1093/jat/5.1.29.
A simplified method for the quantitation of phencyclidine using nitrogen-detection gas chromatography is described. The samples are extracted twice with n-butyl chloride containing benzphetamine as an internal standard. A 0.5 mL sample is required for detection of as little as 5 ng/mL PCP. The assay is easy, fast and reliable. Due to the relatively small volume required, this method is suitable for analysis of pediatric samples.
描述了一种使用氮检测气相色谱法定量苯环己哌啶的简化方法。样品用含苄非他明作为内标的正丁基氯萃取两次。检测低至5 ng/mL的苯环己哌啶需要0.5 mL样品。该测定方法简便、快速且可靠。由于所需体积相对较小，该方法适用于儿科样品的分析。
