Duve R N, Chandra J P, Singh S B
J Assoc Off Anal Chem. 1981 Jul;64(4):1027-9.
The vanadium pentoxide-catalyzed reflux method has been modified to allow open digestion of samples in preparation for determination of organic and inorganic mercury. The reflux digestion performed with a bunsen burner resulted in charred samples, but digestions performed in tubes in a 95-100 degrees C water bath were satisfactory. As many as 40 digestions can be carried out simultaneously, and the technique offers a fast and simple approach to digestion, dilution, and transfer.
五氧化二钒催化回流法已得到改进，以便在测定有机汞和无机汞之前对样品进行开放式消解。用本生灯进行回流消解会导致样品烧焦，但在95 - 100摄氏度水浴中的试管中进行消解效果令人满意。一次可同时进行多达40次消解，该技术为消解、稀释和转移提供了一种快速简便的方法。
