Lafont P, Debeaupuis J P
J Chromatogr. 1980 Oct 24;198(4):481-8. doi: 10.1016/s0021-9673(00)80517-8.
Two methods are proposed for the determination of PR-toxin. One allows a direct quantitative estimation of the mycotoxin, the other utilizes an imine formation after reaction with ammonium hydroxide. In both cases a fluorodensitometric assay on thin-layer chromatographic plates is carried out after spraying with p-dimethylaminobenzaldehyde reagent. The two procedures can be applied to estimate the toxin in foodstuffs at levels as low as 10 and 1 microgram/kg, respectively.