López de Alda-Villaizan M J, García-Falcon S, Lage-Yusty M A, Simal-Lozano J
Universidad de Santiago de Compostela, Facultad de Farmacia, Departamento de Química Analítica, Nutrición, and Bromatología, Spain.
J AOAC Int. 1995 Mar-Apr;78(2):402-6.
We report a quick, simple method for determination of the joint concentration of the 6 polycyclic aromatic hydrocarbons (PAHs) designated by current legislation as quality indicators for drinking water and for surface waters destined for use as drinking water. Water samples are extracted with hexane, and total indicator PAH concentration is determined by synchronous spectrofluorimetry (optimal instrumental parameters are reported). The detection limit (5.0 ng/L), quantitation limit (8.4 ng/L), precision (coefficient of variation, 3.8%), and accuracy (recovery, 77%) were well within the legal bounds for reference methods.
我们报告了一种快速、简便的方法,用于测定6种多环芳烃(PAHs)的联合浓度,这些多环芳烃被现行法规指定为饮用水以及用作饮用水的地表水的质量指标。水样用己烷萃取,通过同步荧光光谱法测定指示性多环芳烃的总浓度(报告了最佳仪器参数)。检测限(5.0 ng/L)、定量限(8.4 ng/L)、精密度(变异系数,3.8%)和准确度(回收率,77%)均在参考方法的法定范围内。