DeSchepper E J, Tate W H, Powers J M
Department of Restorative Dentistry, Indiana University, School of Dentistry, Indianapolis 46202.
Am J Dent. 1993 Oct;6(5):235-8.
The in vitro bond strengths of three resin cements and a light-cured and a laboratory-processed micro-filled composite were measured. Effects of two surface treatments, and three bond enhancers were analyzed. Resin cements were bonded to sandblasted composite substrates, stored at 37 degrees C in 100% humidity overnight, and debonded in tension. An analysis of variance revealed significant differences among bond strengths. Overall, the composite substrate had the largest effect on bond strength, followed by bond enhancer, cement and, finally, surface treatment. Mean bond strengths ranged from 0.9 to 13.6 MPa. A combination of Concept, Dual Cement, phosphoric acid and Silane produced the lowest mean bond strength (0.9 MPa), while EOS, Dual Cement, hydrofluoric acid, and Heliobond produced the highest recorded mean bond strength (13.6 MPa). In general, the highest bonds were produced using the light-cured composite (EOS), the acrylic monomer (Special Bond II) or the dimethacrylate monomer (Heliobond), the adhesive cement (CR Inlay Cement), and surface treatment with hydrofluoric acid (Comp-Etch). Most of the bond failures (86%) with the laboratory-cured microfilled composite were adhesive. With the light-cured composite, 69% of the failures were mixed adhesive-cohesive types.
测量了三种树脂水门汀以及一种光固化和一种实验室加工的微填料复合材料的体外粘结强度。分析了两种表面处理和三种粘结增强剂的效果。将树脂水门汀粘结到喷砂处理的复合材料基底上,在37摄氏度、湿度100%的条件下储存过夜,然后进行拉伸脱粘。方差分析显示粘结强度之间存在显著差异。总体而言,复合材料基底对粘结强度的影响最大,其次是粘结增强剂、水门汀,最后是表面处理。平均粘结强度范围为0.9至13.6兆帕。Concept、双水门汀、磷酸和硅烷的组合产生了最低的平均粘结强度(0.9兆帕),而EOS、双水门汀、氢氟酸和Heliobond产生了记录到的最高平均粘结强度(13.6兆帕)。一般来说,使用光固化复合材料(EOS)、丙烯酸单体(Special Bond II)或二甲基丙烯酸酯单体(Heliobond)、粘结性水门汀(CR Inlay Cement)以及氢氟酸表面处理(Comp-Etch)可产生最高的粘结力。实验室固化的微填料复合材料的大多数粘结失败(86%)是粘结性的。对于光固化复合材料,69%的失败是粘结-内聚混合类型。