Inoue M, Finger W J, Mueller M
Department of Operative Dentistry, Osaka Dental University, Japan.
Am J Dent. 1993 Oct;6(5):243-7.
The present investigation demonstrated that variations in pH between 0.8 and 2.1 and in the duration of etching with an aluminum oxalate/glycine conditioning solution between 5 and 120 seconds has no influence on the retentive strength of restorative polymer to enamel, although the micromorphological appearance of enamel is clearly affected. The lower the pH of and the longer the etching time with the conditioning solution, the more pronounced is the roughness pattern generated. SEM inspection of the fracture sites following debonding of shear bond strength specimens verified consistently cohesive failure in resin close to the interface.
本研究表明,在用草酸铝/甘氨酸预处理溶液进行酸蚀时,pH值在0.8至2.1之间变化,酸蚀时间在5至120秒之间变化,对修复性聚合物与牙釉质的固位强度没有影响,尽管牙釉质的微观形态外观明显受到影响。预处理溶液的pH值越低,酸蚀时间越长,产生的粗糙度模式就越明显。对剪切粘结强度试件脱粘后的断裂部位进行扫描电子显微镜检查,始终证实靠近界面处的树脂发生内聚破坏。