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对与体瓷同时烧制的一种不透明瓷的某些性能进行评估。

Evaluation of some properties of an opaque porcelain fired simultaneously with the body porcelain.

作者信息

O'Brien W J, Boenke K M, Groh C L

机构信息

Department of Biologic and Materials Sciences, School of Dentistry, University of Michigan, Ann Arbor.

出版信息

J Prosthet Dent. 1994 Oct;72(4):414-9. doi: 10.1016/0022-3913(94)90562-2.

Abstract

Recently, a porcelain-fused-to-metal opaque porcelain was introduced that does not require a separate firing before application of the body porcelain. The objective of this study was to determine the properties of this new opaque porcelain and its ability to bond to metal. The properties studied included flexural strength, linear firing shrinkage, coefficient of thermal expansion, powder particle size, and ability to bond to body porcelain and dental alloys. Sintering of this opaque porcelain was complete when fired at 1760 degrees F (960 degrees C) with a linear firing shrinkage of 13.1% +/- 0.2%. No boundary between the opaque and body porcelains could be found with a scanning electron microscope after firing at 1760 degrees F (960 degrees C). The mean flexural strengths were 99 +/- 7 and 101 +/- 8 MPa respectively, for this opaque porcelain and a conventional opaque porcelain, and were not significantly different as assessed with Student's t-test (p = 0.548). The coefficients of thermal expansion for this opaque porcelain was 13.3 +/- 0.2 x 10(-6)/degrees C. Particle size analysis showed a 63% increase in the particles below 5 microns for this opaque porcelain and bonding to two alloys was adequate as indicated by its cohesive failure. Simultaneous firing of this special opaque porcelain and body porcelain produced satisfactory sintering, strength, and bonding to metal.

摘要

最近,一种新型的烤瓷熔附金属用遮色瓷被引入,该遮色瓷在应用体瓷之前无需单独烧制。本研究的目的是确定这种新型遮色瓷的性能及其与金属的结合能力。所研究的性能包括抗弯强度、线性烧成收缩率、热膨胀系数、粉末粒度,以及与体瓷和牙科合金的结合能力。这种遮色瓷在1760华氏度(960摄氏度)烧制时烧结完成,线性烧成收缩率为13.1%±0.2%。在1760华氏度(960摄氏度)烧制后,用扫描电子显微镜未发现遮色瓷与体瓷之间的边界。这种遮色瓷和传统遮色瓷的平均抗弯强度分别为99±7和101±8兆帕,经学生t检验评估差异不显著(p = 0.548)。这种遮色瓷的热膨胀系数为13.3±0.2×10⁻⁶/摄氏度。粒度分析表明,这种遮色瓷中小于5微米的颗粒增加了63%,并且如内聚破坏所示,与两种合金的结合良好。这种特殊遮色瓷与体瓷同时烧制产生了令人满意的烧结效果、强度以及与金属的结合。

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