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Conjugation reactions of cyclodepsipeptide to glutathionyl adducts by direct 'in-beam' synthesis under negative-ion fast-atom bombardment conditions.

作者信息

Loutelier C, Cherton J C, Lange C

机构信息

Département de Chimie, Université de Versailles, France.

出版信息

Rapid Commun Mass Spectrom. 1994 Oct;8(10):844-8. doi: 10.1002/rcm.1290081010.

DOI:10.1002/rcm.1290081010
PMID:8000080
Abstract

The conjugation products of E-destruxin (cyclodepsipeptide) with glutathione have been identified by fast-atom bombardment mass spectrometry. Appropriate conditions were developed for cyclodepsipeptide substrate, which enabled the direct, dynamic mass spectra analysis of spontaneous as well as glutathione-s-transferase catalyzed conjugation reactions. Application to the most active cyclopeptide in the series of destruxins yielded glutathionyl adduct.

摘要

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