Firestone D
U.S. Food and Drug Administration, Division of Pesticides and Industrial Chemicals, Washington, DC 20204.
J AOAC Int. 1994 Jul-Aug;77(4):954-7.
The IUPAC Commission on Oils, Fats and Derivatives undertook development of a method and collaborative study for the determination of triglycerides in vegetable oils by liquid chromatography. Three collaborative studies were conducted from 1985 to 1987. Refinements were made in the method after the first collaborative study, and the second and third collaborative studies demonstrated that the method produces acceptable results. Materials studied were soybean oil, almond oil, sunflower oil, olive oil, rapeseed oil, and blends of palm and sunflower oils, and almond and sunflower oils. Six test samples were analyzed by 18 laboratories from 11 countries in the second study; 4 test samples were analyzed by 16 laboratories from 12 countries in the third study. The method for determination of triglycerides (by partition numbers) in vegetable oils by liquid chromatography was adopted first action by AOAC INTERNATIONAL as an IUPAC-AOCS-AOAC method.
国际纯粹与应用化学联合会（IUPAC）油脂及衍生物委员会开展了一项关于用液相色谱法测定植物油中甘油三酯的方法开发及协作研究。1985年至1987年进行了三项协作研究。在首次协作研究后对方法进行了改进，第二次和第三次协作研究表明该方法能产生可接受的结果。所研究的材料有大豆油、杏仁油、葵花籽油、橄榄油、菜籽油，以及棕榈油与葵花籽油的混合物、杏仁油与葵花籽油的混合物。在第二项研究中，来自11个国家的18个实验室分析了6个测试样品；在第三项研究中，来自12个国家的16个实验室分析了4个测试样品。用液相色谱法测定植物油中甘油三酯（通过分配数）的方法被AOAC INTERNATIONAL首次采用，作为一种IUPAC - AOCS - AOAC方法。
