Rezvukhin A I, Shalaurova I Iu, Potapova I A, Aliab'eva I A
Vopr Med Khim. 1993 Sep-Oct;39(5):55-8.
Complete analysis of blood serum free fatty acids was carried out after methylation of the acids in the mixture containing methanol-acetyl chloride 50:1 and subsequent evaluation of their methyl esters using a gas chromatography analyser. Standard mixtures of free fatty acids and their methyl esters were analyzed before study of blood serum free fatty acids; composition of fish-liver oil (Far Eastern mackerel), containing definite fatty acids was also studied. Combination of gas chromatography and mass spectrometry enabled to identify all the free fatty acids and to detect their main characteristics (time of retention, typical mass spectrum).
在含有甲醇 - 乙酰氯（比例为50:1）的混合物中对酸进行甲基化后，对血清游离脂肪酸进行了全面分析，随后使用气相色谱分析仪对其甲酯进行评估。在研究血清游离脂肪酸之前，先对游离脂肪酸及其甲酯的标准混合物进行了分析；还研究了含有特定脂肪酸的鱼肝油（远东鲭鱼）的成分。气相色谱和质谱联用能够鉴定所有游离脂肪酸并检测其主要特征（保留时间、典型质谱）。
