关于假定的相容性溶质5-二甲基磺酰基戊酸酯是一种提取假象的证据。
Evidence that the putative compatible solute 5-dimethylsulfoniopentanoate is an extraction artifact.
作者信息
Hanson A D, Huang Z H, Gage D A
机构信息
Institut de Recherche en Biologie Végétale de l'Université de Montréal, Québec, Canada.
出版信息
Plant Physiol. 1993 Apr;101(4):1391-3. doi: 10.1104/pp.101.4.1391.
Abstract
A novel gas chromatography-mass spectrometry method for analyzing sulfonium compounds as their S-demethylated silyl derivatives has clarified the origin of 5-dimethylsulfoniopentanoate. This compound, previously reported from flowers of Diplotaxis tenuifolia (L.) DC. (Cruciferae), is generated from glucoerucin during treatment with hot 6 N HCl. Glucoerucin is the characteristic glucosinolate of D. tenuifolia.
摘要
一种用于分析锍化合物的新型气相色谱-质谱法，将锍化合物作为其S-去甲基化硅烷基衍生物进行分析，该方法阐明了5-二甲基磺酰基戊酸酯的来源。这种化合物先前在细裂双行芥（十字花科）的花中被报道过，它是在热6N盐酸处理过程中由葡糖芥苷产生的。葡糖芥苷是细裂双行芥的特征硫代葡萄糖苷。
相似文献
1
Evidence that the putative compatible solute 5-dimethylsulfoniopentanoate is an extraction artifact.关于假定的相容性溶质5-二甲基磺酰基戊酸酯是一种提取假象的证据。
Plant Physiol. 1993 Apr;101(4):1391-3. doi: 10.1104/pp.101.4.1391.
2
Comprehensive chromatographic and spectroscopic methods for the separation and identification of intact glucosinolates.用于完整硫代葡萄糖苷分离与鉴定的综合色谱和光谱方法。
Anal Biochem. 1996 Aug 1;239(2):168-79. doi: 10.1006/abio.1996.0312.
3
Basic theory of mass spectrometry.质谱分析的基本理论。
Clin Chim Acta. 1995 Oct-Nov;241-242:15-71.
4
Tandem mass spectrometry of glycolipids.
Methods Enzymol. 1990;193:738-68. doi: 10.1016/0076-6879(90)93448-t.
5
Systematic study of high molecular weight compounds in Amazonian plants by high temperature gas chromatography-mass spectrometry.利用高温气相色谱-质谱联用技术对亚马逊植物中的高分子量化合物进行系统研究。
Z Naturforsch C J Biosci. 2000 Mar-Apr;55(3-4):175-9. doi: 10.1515/znc-2000-3-407.
6
A multi-analytical platform based on pressurized-liquid extraction, in vitro assays and liquid chromatography/gas chromatography coupled to high resolution mass spectrometry for food by-products valorisation. Part 2: Characterization of bioactive compounds from goldenberry (Physalis peruviana L.) calyx extracts using hyphenated techniques.基于加压液体萃取、体外测定和液相色谱/气相色谱-高分辨质谱联用的多分析平台用于食品副产物增值利用。第 2 部分：使用联用技术对灯笼果（Physalis peruviana L.）花萼提取物中的生物活性化合物进行表征。
J Chromatogr A. 2019 Jan 11;1584:144-154. doi: 10.1016/j.chroma.2018.11.054. Epub 2018 Nov 24.
7
Microwave distillation followed by headspace single drop microextraction coupled to gas chromatography-mass spectrometry (GC-MS) for fast analysis of volatile components of Echinophora platyloba DC.采用微波蒸馏结合顶空单滴微萃取，与气相色谱-质谱联用（GC-MS），快速分析蓝刺头中挥发性成分。
Food Chem. 2013 May 1;138(1):251-5. doi: 10.1016/j.foodchem.2012.09.112. Epub 2012 Nov 8.
8
Constituents in Easter lily flowers with medicinal activity.具有药用活性的复活节百合花中的成分。
Life Sci. 2004 Dec 24;76(6):671-83. doi: 10.1016/j.lfs.2004.10.001.
9
Cardioprotective potential of Irish macroalgae: generation of glycine betaine and dimethylsulfoniopropionate containing extracts by accelerated solvent extraction.
Planta Med. 2015 Jun;81(8):679-84. doi: 10.1055/s-0035-1546018. Epub 2015 May 27.
10
Negative ion fast atom bombardment and collision-induced dissociation mass spectrometry of the 2-, 3-, 4- and 6-deoxy derivatives from methyl beta-D-galactopyranoside and related compounds.β-D-吡喃半乳糖甲基苷及相关化合物的2-、3-、4-和6-脱氧衍生物的负离子快原子轰击和碰撞诱导解离质谱分析
Biol Mass Spectrom. 1994 Dec;23(12):764-70. doi: 10.1002/bms.1200231208.
本文引用的文献
1
Analysis of acylcarnitines as their N-demethylated ester derivatives by gas chromatography-chemical ionization mass spectrometry.通过气相色谱-化学电离质谱法分析酰基肉碱作为其N-去甲基酯衍生物。
Anal Biochem. 1991 Nov 15;199(1):98-105. doi: 10.1016/0003-2697(91)90275-x.
Zotero 插件