Kalashnikov V M, Zaĭchik V E
Vopr Med Khim. 1977 Jan-Feb(1):122-7.
A method of instrumental photonuclear activational analysis is developed for estimation of nitrogen, fluorine and phosphorus in bone tissue samples. The irradiation with maximal energy 15.6 MeV, obtained on linear accelerator of electrons LUE-25 RIMR AMN USSR, was used for activation. Estimations were carried out by the relative method with recording the intensity of positron radiation of 13N, 18F and 30P in samples and standards by means of device for gamma-gamma-coincidence. In chosen regimens of the analysis the statistical errors of nitrogen and phosphorus estimation did not esceed 1.5%, of fluorine-5%; the sensitivity of the method for nitrogen was found to be 0.06% for fluorine-0.006%, for phosphorus-0.12%; on analysis of recovery the relative standard deviation in results accounted for nitrogen-5.4%, for fluorine-6.7% for phosphorus 6.2%. Correctness in concentrations of the elements, estimated by the method described, correlated with the data, obtained in activation with reactor neutrons and with 14MeV generator neutrons.
开发了一种仪器光子核活化分析方法,用于估算骨组织样本中的氮、氟和磷。使用苏联医学科学院放射医学研究所LUE - 25型电子直线加速器产生的最大能量为15.6 MeV的辐射进行活化。通过相对法进行估算,借助伽马 - 伽马符合装置记录样本和标准品中¹³N、¹⁸F和³⁰P的正电子辐射强度。在选定的分析方案中,氮和磷估算的统计误差不超过1.5%,氟的为5%;该方法对氮的灵敏度为0.06%,对氟为0.006%,对磷为0.12%;在回收率分析中,结果的相对标准偏差氮为5.4%,氟为6.7%,磷为6.2%。用所述方法估算的元素浓度的准确性与用反应堆中子和14 MeV发生器中子活化获得的数据相关。