Tymes N W
J Chromatogr Sci. 1977 May 10;15(5):151-5. doi: 10.1093/chromsci/15.5.151.
High-performance reverse-phase liquid chromatographic data on 28 corticoids and related steroid analogs, plus methyl and propyl parabens, are presented. Retention values, relative to acetone, are reported for each steroid on Bondapak Phenyl/Corasil, Bondapak C18/Corasil, and micro(micron) Bondapak C18 columns, and methanol/water or acetonitrile/water mobile phases. Ultraviolet detector response data for four of the steroids and calculated efficiencies for the three different reverse-phase columns are given. Chromatograms showing the separations of four steroids plus methyl and propyl parabens obtained on each of the three columns are also presented.
本文给出了28种皮质类固醇及相关甾体类似物，以及对羟基苯甲酸甲酯和对羟基苯甲酸丙酯的高效反相液相色谱数据。报告了每种甾体在Bondapak苯基/硅胶、Bondapak C18/硅胶和微（微米）Bondapak C18柱上，相对于丙酮的保留值，以及甲醇/水或乙腈/水流动相。给出了四种甾体的紫外检测器响应数据，以及三种不同反相柱的计算塔板数。还给出了在三根柱上分别得到的四种甾体以及对羟基苯甲酸甲酯和对羟基苯甲酸丙酯的分离色谱图。
