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能量过滤高分辨率电子显微镜和成分敏感成像。

Energy-filtered high-resolution electron microscopy and composition-sensitive imaging.

作者信息

Wang Z L

机构信息

School of Materials Science and Engineering, Georgia Institute of Technology, Atlanta 30332-0245, USA.

出版信息

Microsc Res Tech. 1996 Feb 15;33(3):279-87. doi: 10.1002/(SICI)1097-0029(19960215)33:3<279::AID-JEMT5>3.0.CO;2-L.

Abstract

Energy-filtered electron imaging is one of the future directions of high-resolution electron microscopy (HREM). In this paper, characteristics and applications of energy-selected HREM are illustrated. Image contrast can be dramatically improved with the use of an energy filter. High-resolution chemical-sensitive imaging using ionization edge loss electrons is demonstrated in studies on Ni/Ti and A1/Ti multilayer thin films. It has been shown that the spatial resolution of energy-selected ionization edge electron images is dominated by the signal-to-noise ratio. Experimental parameters which may be selected to improve the signal-to-noise ratio are discussed. It is pointed out that since the width of the energy-selecting window is small, the energy-filtered ionization edge electron image is sensitive to the specimen composition, but the calculation of the specimen composition based on the energy-filtered images relies on the integrated ionization cross-sections which are largely determined by the solid state effects. Therefore, the energy-filtered ionization image should be referred as composition-sensitive image rather than compositional image.

摘要

能量过滤电子成像技术是高分辨率电子显微镜(HREM)未来的发展方向之一。本文阐述了能量选择高分辨率电子显微镜的特点与应用。使用能量过滤器可显著提高图像对比度。在对镍/钛和铝/钛多层薄膜的研究中,展示了利用电离边损失电子进行的高分辨率化学敏感成像。研究表明,能量选择电离边电子图像的空间分辨率受信噪比主导。文中讨论了可用于提高信噪比的实验参数。需要指出的是,由于能量选择窗口宽度较小,能量过滤电离边电子图像对样品成分敏感,但基于能量过滤图像计算样品成分依赖于积分电离截面,而这在很大程度上由固态效应决定。因此,能量过滤电离图像应称为成分敏感图像而非成分图像。

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