Merli P G, Migliori A, Nacucchi M, Vittor Antisari M
CNR-Istituto LAMEL, Bologna, Italy.
Ultramicroscopy. 1996 Sep;65(1-2):23-30. doi: 10.1016/s0304-3991(96)00053-8.
Comparative studies on the ultimate spatial resolution of the Scanning Electron Microscope, using different components of the electron signal have been performed on specimens providing compositional contrast. By operating the microscope in conventional way as well as with a specifically designed set-up we have ascertained that the delocalized components of the signal provide a spatial resolution of the order of the beam size, even if the practical use can be limited by the noise. To amplify the contribution of the delocalized components of the signal, as backscattered electrons by a bulk specimen or forward scattered electrons by a thin specimen, we used a device consisting of a plate of a material with high secondary yield placed above or below the sample. An important practical implication arises from this study. A detecting system consisting of a standard Everhart-Thornley detector coupled with a converter of backscattered or transmitted electrons represents a high performance detecting device for low voltage observations.
利用电子信号的不同成分,对扫描电子显微镜的最终空间分辨率进行了比较研究,研究对象为具有成分对比度的标本。通过以传统方式操作显微镜以及采用专门设计的装置,我们已确定,即使实际应用可能受到噪声限制,信号的离域成分仍能提供与束斑尺寸相当的空间分辨率。为了增强信号离域成分的贡献,如大块标本的背散射电子或薄标本的前向散射电子,我们使用了一种装置,该装置由一块置于样品上方或下方的具有高二次电子产额的材料板组成。这项研究产生了一个重要的实际意义。由标准的埃弗哈特 - 索恩利探测器与背散射或透射电子转换器组成的检测系统,是用于低电压观察的高性能检测装置。