Finger W J, Uno S
Department of Prosthetic Dentistry and Dental Materials Science, Dental School, RWTH, Aachen, Germany.
Am J Dent. 1996 Feb;9(1):27-30.
To investigate the effects of acetone or water based Gluma primers on bonding efficacy when applied to acid-etched wet, dry or rewetted dentin.
Shear bond strength (SBS, 24 hours) was measured on human dentin etched with 20% phosphoric acid gel and rinsed with water in the wet (blot dried), the conventional (2 seconds air blast), the dry (10 seconds air drying), and the rewetted stage (10 seconds air drying, remoistening and blot drying). The priming solution was either the original water based or an acetone based experimental Gluma primer. Cavity sealing performance and depth of resin impregnation were determined by solvent and by technique along the margins of 4.5 mm wide cylindrical dentin cavities with 90 degree cavosurface angle.
The SBSs of the wet technique groups were approximately 18 MPa, irrespective of the primer solvent. Conventional drying gave an SBS almost as high (16.5 MPa). Rewetting was highly effective with acetone as the primer solvent. The dry techniques resulted in moderate (water) and poor (acetone) bond strengths. The cavity margins of acetone based primer treated specimens were consistently gap free with the wet technique. The other seven groups showed between two and six gaps in each group of six specimens. The resin impregnated layer (RIL) thicknesses were 12.5 microns approximately in the wet groups, and thus identical with the total depth of demineralization resulting from the 30-second etching. The alternative techniques showed significantly thinner RILs particularly in the dry groups (7.5 microns).
研究丙酮基或水基Gluma底漆应用于酸蚀后的湿、干或再湿牙本质时对粘结效果的影响。
在用人牙本质用20%磷酸凝胶酸蚀并用水冲洗后的湿(吸干)、常规(2秒气吹)、干(10秒气干)和再湿阶段(10秒气干、再湿润并吸干)条件下,测量剪切粘结强度(SBS,24小时)。底漆溶液为原始水基或丙酮基实验性Gluma底漆。通过溶剂并沿90度洞缘角的4.5毫米宽圆柱形牙本质洞边缘的技术来测定窝洞封闭性能和树脂浸渍深度。
无论底漆溶剂如何,湿技术组的SBS约为18兆帕。常规干燥得到的SBS几乎同样高(16.5兆帕)。以丙酮作为底漆溶剂时,再湿润非常有效。干技术导致中等(水基)和较差(丙酮基)的粘结强度。用丙酮基底漆处理的标本的窝洞边缘在湿技术下始终无间隙。其他七组在每组六个标本中显示出两到六个间隙。湿组的树脂浸渍层(RIL)厚度约为12.5微米,因此与30秒蚀刻产生的脱矿总深度相同。替代技术显示RIL明显更薄,特别是在干组(7.5微米)。