烯丙基二甲基甲硅烷基醚作为类固醇衍生物用于气相色谱-质谱分析的评估
Evaluation of allyldimethylsilyl ethers as steroid derivatives for gas chromatography-mass spectrometry.
作者信息
Blair I A, Phillipou G
出版信息
J Chromatogr Sci. 1977 Oct;15(10):478-9. doi: 10.1093/chromsci/15.10.478.
PMID:914966
Abstract
The preparation of allyldimethysilyl steroid ethers for the analysis of steroids by GC-MS has been studied in depth. The application of these derivatives is shown to be unsatisfactory due to competitive formation of allylsiloxane derivatives.
摘要
对用于气相色谱-质谱联用仪分析甾体化合物的烯丙基二甲基硅基甾体醚的制备进行了深入研究。结果表明，由于烯丙基硅氧烷衍生物的竞争性生成，这些衍生物的应用并不理想。
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