• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利:CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验

[固相萃取法在红外光谱法鉴定未知物质中用于样品制备的应用]

[The use of a method of solid-phase extraction for sample preparation in the identification of unknown substances by IR spectroscopy].

作者信息

Beliaev A V, Sorokin V I, Orlova O S, Kimstach T B

出版信息

Sud Med Ekspert. 1997 Jul-Sep;40(3):23-8.

PMID:9304249
Abstract

Identification of synthetic narcotics is difficult because they do not possess any apparent individual signs and the specimens are contaminated with various fillers and additives, which rules out investigations by infrared spectroscopy, widely used in expert practice. Use of solid-phase extraction during preparation of samples helps prepare highly purified samples which can be further identified by IR spectroscopy. The authors present the protocol of identification of unknown substances and recognition of narcotics and describe methods for identification of some confiscated narcotics (methadone, MDA, phencyclidine, methaqualone, codeine, ethylmorphine, cocaine, etc.).

摘要

合成麻醉品的鉴定很困难,因为它们没有任何明显的个体特征,而且样本被各种填充剂和添加剂污染,这排除了在专家实践中广泛使用的红外光谱法进行调查的可能性。在样品制备过程中使用固相萃取有助于制备高纯度样品,这些样品可通过红外光谱法进一步鉴定。作者介绍了未知物质的鉴定方案和麻醉品的识别方法,并描述了一些查获的麻醉品(美沙酮、MDA、苯环己哌啶、甲喹酮、可待因、乙基吗啡、可卡因等)的鉴定方法。

相似文献

1
[The use of a method of solid-phase extraction for sample preparation in the identification of unknown substances by IR spectroscopy].[固相萃取法在红外光谱法鉴定未知物质中用于样品制备的应用]
Sud Med Ekspert. 1997 Jul-Sep;40(3):23-8.
2
Classification of narcotics in solid mixtures using principal component analysis and Raman spectroscopy.使用主成分分析和拉曼光谱法对固体混合物中的麻醉药品进行分类
J Forensic Sci. 2002 Mar;47(2):275-84.
3
[The use of derivative spectrophotometry for the identification of drug and narcotic substances extracted from biological objects].
Sud Med Ekspert. 1992 Jan-Mar;35(1):19-22.
4
[Example for a new alternative application of NIR spectroscopy in the parallel determination of active ingredients and an excipient in powders and tablets].[近红外光谱法在粉末和片剂中活性成分与辅料平行测定新的替代应用示例]
Acta Pharm Hung. 2005;75(3):141-5.
5
The extraction and infrared identification of gamma-hydroxybutyric acid (GHB) from aqueous solutions.从水溶液中提取γ-羟基丁酸(GHB)并进行红外鉴定。
J Forensic Sci. 2004 Jan;49(1):52-9.
6
[The isolation and determination of different narcotic and drug substances after the acid hydrolysis of biological material. (1)].生物材料酸水解后不同麻醉和药物物质的分离与测定。(1)
Sud Med Ekspert. 1998 Nov-Dec;41(6):26-7.
7
Some advances in Fourier transform infrared transflection analysis and potential applications in forensic chemistry.傅里叶变换红外漫反射分析的一些进展及其在法医化学中的潜在应用。
Appl Spectrosc. 2009 May;63(5):507-11. doi: 10.1366/000370209788346887.
8
Preparation and usage of a new solid phase micro-extraction membrane.一种新型固相微萃取膜的制备与应用
Forensic Sci Int. 2004 Jan 28;139(2-3):177-81. doi: 10.1016/j.forsciint.2003.10.020.
9
Variable temperature infrared spectroscopy: a convenient tool for studying the thermodynamics of weak solid-gas interactions.可变温度红外光谱法:研究弱固-气相互作用热力学的便捷工具。
Chem Soc Rev. 2005 Oct;34(10):846-57. doi: 10.1039/b407049f. Epub 2005 Aug 23.
10
Optimization of extraction and separation of narcotics from urine.尿液中麻醉药品提取与分离的优化。
Clin Biochem. 1974 Sep;7(3):280-9. doi: 10.1016/s0009-9120(74)92378-9.