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高效液相色谱法对药物剂型中苯酚和间苯二酚的定量测定。

Quantitative determinations of phenol and resorcinol in pharmaceutical dosage forms by high-pressure liquid chromatography.

作者信息

Das Gupta V

出版信息

J Pharm Sci. 1976 Nov;65(11):1706-7. doi: 10.1002/jps.2600651139.

DOI:10.1002/jps.2600651139
PMID:994010
Abstract

The quantitative determinations of phenol in phenolated calamine lotion USP and of phenol and resorcinol in phenol-resorcinol-boric acid solution by high-pressure liquid chromatography are reported. The procedures are simple, rapid (no special preliminary treatment is required), and accurate. There is no interference from other ingredients of the lotion (bentonite magma, calamine, and zinc oxide) or solution (acetone and boric acid).

摘要

本文报道了采用高压液相色谱法对美国药典含酚炉甘石洗剂中的苯酚以及苯酚 - 间苯二酚 - 硼酸溶液中的苯酚和间苯二酚进行定量测定。该方法操作简单、快速（无需特殊预处理）且准确。洗剂中的其他成分（膨润土岩浆、炉甘石和氧化锌）或溶液中的其他成分（丙酮和硼酸）均无干扰。

相似文献

1
Quantitative determinations of phenol and resorcinol in pharmaceutical dosage forms by high-pressure liquid chromatography.高效液相色谱法对药物剂型中苯酚和间苯二酚的定量测定。
J Pharm Sci. 1976 Nov;65(11):1706-7. doi: 10.1002/jps.2600651139.
2
Quantitative determination of resorcinal and phenol in resorcinol-phenol-boric acid solution.
J Pharm Sci. 1974 Jan;63(1):93-5. doi: 10.1002/jps.2600630124.
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Quantitative determination of phenol by high-pressure liquid chromatography.
J Pharm Sci. 1977 Aug;66(8):1201-2. doi: 10.1002/jps.2600660840.
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Quantitative determination of phenol in phenolated calamine lotion USP.美国药典中含酚炉甘石洗剂中苯酚的定量测定。
J Pharm Sci. 1975 Jul;64(7):1199-200. doi: 10.1002/jps.2600640715.
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[Synchronous fluorescent determination of phenol and resorcinol using linear regression of multiwavelength data].[基于多波长数据线性回归的苯酚和间苯二酚同步荧光测定法]
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Kinetic fluorimetric measurement of trace resorcinol in phenol mixtures.苯酚混合物中痕量间苯二酚的动力学荧光测定法
J Fluoresc. 2007 Jan;17(1):113-8. doi: 10.1007/s10895-006-0128-2. Epub 2006 Sep 22.
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Determination of phenol and resorcinol using 1,3-dibromo-5,5-dimethylhydantoin (DBH) analogous to the Koppeschaar reaction. Analytical methods of pharmacopoeias with DBH in respect to environmental and economical concern, Part 6.采用类似于科佩沙尔反应的1,3 - 二溴 - 5,5 - 二甲基海因（DBH）测定苯酚和间苯二酚。从环境和经济角度考量，药典中使用DBH的分析方法，第6部分。
Pharmazie. 2001 Oct;56(10):777-9.
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Determination of phenol in the presence of resorcinol applying substitution with excess bromine water; structure of the bromination products.
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Quantitative determination of resorcinol in presence of phenol.在苯酚存在的情况下对间苯二酚进行定量测定。
J Pharm Sci. 1976 Jan;65(1):144-5. doi: 10.1002/jps.2600650138.
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Hydroxylation and conjugation of phenol by the frog Rana temporaria.
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Quantitative Analysis of Resorcinol from Marketed Hair Tonic Using Liquid Chromatographic Technique.采用液相色谱技术对市售生发水间苯二酚进行定量分析。
Int Sch Res Notices. 2014 Sep 2;2014:632591. doi: 10.1155/2014/632591. eCollection 2014.
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Simultaneous Quantification of Dexpanthenol and Resorcinol from Hair Care Formulation Using Liquid Chromatography: Method Development and Validation.使用液相色谱法同时定量测定护发配方中的泛醇和间苯二酚：方法开发与验证
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