Yilmaz H, Dinçer C
Department of Prosthodontics, Gazi University Faculty of Dentistry, Ankara, Turkey.
J Dent. 1999 Mar;27(3):215-22. doi: 10.1016/s0300-5712(98)00045-1.
The aim of this study was to investigate the bond compatibility between porcelain and titanium, by using three-point bending, oxide adherence and thermal expansion tests, and to compare the results with those of a conventional NiCr alloy-porcelain system.
The three-point bending test was used and the results were evaluated according to DIN draft 13927. Fractured surfaces of the metal and porcelain were examined macroscopically. The oxide adherence test was applied to titanium and NiCr alloy with appropriate oxidation degrees. After an oxide film was formed on the specimens, tensile strength test was applied. Oxide adherence strength values were set and fractured surfaces were examined macroscopically. In the thermal expansion test, thermal expansion curves and thermal expansion coefficients of titanium, NiCr alloy and tested porcelains were determined. Differences in thermal expansion values (delta alpha) in all metal-porcelain pairs were calculated to allow inferences to be made about residual stress levels.
The bending strengths of all groups were found to be within the acceptable standard levels. At the end of the oxide adherence test, the results indicated that the adherence of the formed oxides to the metals were at a desired level. As a result of the thermal expansion test, the titanium-porcelain and NiCr-porcelain systems showed compressive thermal stress. However, the titanium-porcelain pair exhibited large positive delta alpha values. This results is found to be above the proposed thermal compatibility.
It was concluded that the bond compatibility between titanium and porcelain was comparable with the NiCr-porcelain system.
本研究旨在通过三点弯曲试验、氧化物附着力试验和热膨胀试验,研究瓷与钛之间的结合相容性,并将结果与传统镍铬合金 - 瓷系统的结果进行比较。
采用三点弯曲试验,并根据DIN草案13927对结果进行评估。对金属和瓷的断裂表面进行宏观检查。对具有适当氧化程度的钛和镍铬合金进行氧化物附着力试验。在试样上形成氧化膜后,进行拉伸强度试验。设定氧化物附着力强度值,并对断裂表面进行宏观检查。在热膨胀试验中,测定钛、镍铬合金和受试瓷的热膨胀曲线和热膨胀系数。计算所有金属 - 瓷对的热膨胀值差异(δα)以便推断残余应力水平。
发现所有组的弯曲强度均在可接受的标准水平内。在氧化物附着力试验结束时,结果表明形成的氧化物与金属的附着力处于理想水平。热膨胀试验的结果表明,钛 - 瓷和镍铬 - 瓷系统表现出压缩热应力。然而,钛 - 瓷对表现出较大的正δα值。该结果高于建议的热相容性。
得出结论,钛与瓷之间的结合相容性与镍铬 - 瓷系统相当。