以十二烷基硫酸钠以及β-环糊精与牛磺脱氧胆酸的混合物作为手性选择剂，采用胶束电动色谱法（MEKC）对硒氨基酸衍生物进行对映体拆分。 - Suppr

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Enantiomeric resolution of selenoamino acid derivatives by micellar electrokinetic chromatography (MEKC) with sodium dodecyl sulphate and a mixture of beta-cyclodextrin and taurodeoxycholic acid as chiral selectors.

作者信息

Pérez Méndez S, Blanco González E, Sanz-Medel A

机构信息

Department of Physical and Analytical Chemistry, University of Oviedo, C/ Julián Clavería, 8, 33006-Oviedo, Spain.

出版信息

Biomed Chromatogr. 2000 Feb;14(1):8-9. doi: 10.1002/(SICI)1099-0801(200002)14:1<8::AID-BMC946>3.0.CO;2-W.

DOI:10.1002/(SICI)1099-0801(200002)14:1<8::AID-BMC946>3.0.CO;2-W

PMID:10664549

Abstract

摘要

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Enantiomeric resolution of selenoamino acid derivatives by micellar electrokinetic chromatography (MEKC) with sodium dodecyl sulphate and a mixture of beta-cyclodextrin and taurodeoxycholic acid as chiral selectors.

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Enantiomeric resolution of selenoamino acid derivatives by micellar electrokinetic chromatography (MEKC) with sodium dodecyl sulphate and a mixture of beta-cyclodextrin and taurodeoxycholic acid as chiral selectors.

作者信息

Pérez Méndez S, Blanco González E, Sanz-Medel A

机构信息

Department of Physical and Analytical Chemistry, University of Oviedo, C/ Julián Clavería, 8, 33006-Oviedo, Spain.

出版信息

Biomed Chromatogr. 2000 Feb;14(1):8-9. doi: 10.1002/(SICI)1099-0801(200002)14:1<8::AID-BMC946>3.0.CO;2-W.

DOI:10.1002/(SICI)1099-0801(200002)14:1<8::AID-BMC946>3.0.CO;2-W

PMID:10664549

Abstract

摘要

相似文献

Biomed Chromatogr. 2000 Feb;14(1):8-9. doi: 10.1002/(SICI)1099-0801(200002)14:1<8::AID-BMC946>3.0.CO;2-W.

Chiral separation of amino acid esters by micellar electrokinetic chromatography.

Electrophoresis. 2001 Sep;22(15):3291-6. doi: 10.1002/1522-2683(200109)22:15<3291::AID-ELPS3291>3.0.CO;2-A.

Enantiomeric separation of amino acids derivatized with fluoresceine isothiocyanate isomer I by micellar electrokinetic chromatography using beta- and gamma-cyclodextrins as chiral selectors.

Electrophoresis. 1999 Jun;20(7):1538-45. doi: 10.1002/(SICI)1522-2683(19990601)20:7<1538::AID-ELPS1538>3.0.CO;2-1.

Determination of the enantiomeric purity of N-propionyl-6,7-dimethoxy-2-aminotetralin by cyclodextrin-modified micellar electrokinetic chromatography.

Electrophoresis. 1997 Jun;18(6):996-1001. doi: 10.1002/elps.1150180622.

Chiral separation of vinpocetine using cyclodextrin-modified micellar electrokinetic chromatography.

Chirality. 2012 Mar;24(3):252-4. doi: 10.1002/chir.21990. Epub 2012 Jan 24.

High selectivity in new chiral separations of dansyl amino acids by cyclodextrin derivatives in electrokinetic chromatography.

J Chromatogr A. 2007 Jul 6;1155(2):172-9. doi: 10.1016/j.chroma.2007.02.006. Epub 2007 Feb 8.

Fast enantiomeric separation of basis drugs by electrokinetic chromatography. Application to the quantitation of terbutaline in a pharmaceutical preparation.

Electrophoresis. 2001 Sep;22(15):3191-7. doi: 10.1002/1522-2683(200109)22:15<3191::AID-ELPS3191>3.0.CO;2-G.

Separation of chiral amino acids by micellular electrokinetic chromatography with derivatized cyclodextrins.

Biomed Chromatogr. 1997 Jul-Aug;11(4):230-5. doi: 10.1002/(SICI)1099-0801(199707)11:4<230::AID-BMC678>3.0.CO;2-2.

Delta-cyclodextrin as novel chiral probe for enantiomeric separation by electromigration methods.

Electrophoresis. 2006 Nov;27(21):4359-63. doi: 10.1002/elps.200600284.

Enantiomeric separation of a group of chiral dihydropyridines by electrokinetic chromatography.

Electrophoresis. 2000 May;21(8):1565-73. doi: 10.1002/(SICI)1522-2683(20000501)21:8<1565::AID-ELPS1565>3.0.CO;2-2.