Theobald A, Simoneau C, Hannaert P, Roncari P, Roncari A, Rudolph T, Anklam E
European Commission, DG-Joint Research Centre, Institute for Health and Consumer Protection, Ispra, Va., Italy.
Food Addit Contam. 2000 Oct;17(10):881-7. doi: 10.1080/026520300420475.
The levels of bisphenol-F-diglycidyl ether (BFDGE) were quantified as part of a European survey on the migration of residues of epoxy resins into oil from canned fish. The contents of BFDGE in cans, lids and fish collected from all 15 Member States of the European Union and Switzerland were analysed in 382 samples. Cans and lids were separately extracted with acetonitrile. The extraction from fish was carried out with hexane followed by re-extraction with acetonitrile. The analysis was performed by reverse phase HPLC with fluorescence detection. BFDGE could be detected in 12% of the fish, 24% of the cans and 18% of the lids. Only 3% of the fish contained BFDGE in concentrations considerably above 1 mg/kg. In addition to the presented data, a comparison was made with the levels of BADGE (bisphenol-A-diglycidyl ether) analysed in the same products in the context of a previous study.
作为一项关于环氧树脂残留物向罐装鱼中的油迁移的欧洲调查的一部分,对双酚F - 二缩水甘油醚(BFDGE)的含量进行了定量分析。对从欧盟所有15个成员国和瑞士收集的罐头、盖子和鱼中的BFDGE含量进行了分析,共382个样本。罐头和盖子分别用乙腈萃取。鱼的萃取先用己烷进行,然后再用乙腈重新萃取。分析采用反相高效液相色谱法并进行荧光检测。在12%的鱼、24%的罐头和18%的盖子中可检测到BFDGE。只有3%的鱼所含BFDGE浓度大大高于1毫克/千克。除了所呈现的数据外,还将其与先前一项研究中对相同产品分析的双酚A - 二缩水甘油醚(BADGE)含量进行了比较。