日本市场上罐装食品和即饮咖啡中双酚A二缩水甘油醚（BADGE）和双酚F二缩水甘油醚（BFDGE）的氯醇
Chlorohydrins of bisphenol A diglycidyl ether (BADGE) and of bisphenol F diglycidyl ether (BFDGE) in canned foods and ready-to-drink coffees from the Japanese market.
作者信息
Uematsu Y, Hirata K, Suzuki K, Iida K, Saito K
机构信息
Tokyo Metropolitan Research Laboratory of Public Health, Japan.
出版信息
Food Addit Contam. 2001 Feb;18(2):177-85. doi: 10.1080/02652030010005501.
BADGE.2HCl and BFDGE.2HCl were determined in 28 samples of ready-to-drink canned coffee and 18 samples of canned vegetables (10 corn, 5 tomatoes and 3 others), all from the Japanese market. HPLC was used as the principal analytical method and GC-MS for confirmation of relevant LC fractions. BADGE.2HCl was found to be present in one canned coffee and five samples of corn, BFDGE.2HCl in four samples of canned tomatoes and in one canned corn. No sample was found which exceeded the 1 mg/kg limit of the EU for the BADGE chlorohydrins. However the highest concentration was found for the sum of BFDGE.2HCl anti BFDGE.HCl.H2O at a level of 1.5 mg/kg. A Beilstein test confirmed that all cans containing foods contaminated with BADGE.2HCl or BFDGE.2HCl had at lest one part coated with a PVC organosol.
对来自日本市场的28份即饮罐装咖啡样品和18份罐装蔬菜样品（10份玉米、5份番茄和3份其他蔬菜）进行了BADGE.2HCl和BFDGE.2HCl的检测。采用高效液相色谱法（HPLC）作为主要分析方法，气相色谱 - 质谱联用法（GC - MS）用于确认相关液相色谱馏分。在一份罐装咖啡和五份玉米样品中发现了BADGE.2HCl，在四份罐装番茄样品和一份罐装玉米中发现了BFDGE.2HCl。未发现任何样品超过欧盟对BADGE氯醇的1毫克/千克限量。然而，BFDGE.2HCl和BFDGE.HCl.H2O总和的最高浓度为1.5毫克/千克。贝尔斯坦试验证实，所有含有被BADGE.2HCl或BFDGE.2HCl污染食品的罐头至少有一部分涂有聚氯乙烯有机溶胶。
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