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二 - μ - 羟基 - 双（二异丙基镓）- 1,4,8,11 - 四甲基 - 1,4,8,11 - 四氮杂环十四烷（1/1）

Di-&mgr;-hydroxo-bis(diisopropylgallium)-1,4,8,11-tetramethyl-1,4,8, 11-tetraazacyclotetradecane (1/1).

作者信息

Boag NM, Coward KM, Jones AC, Pemble ME, Thompson JR

机构信息

Department of Chemistry, University of Salford, Salford M5 4WT, England.

出版信息

Acta Crystallogr C. 2000 Dec;56 (Pt 12):1438-9. doi: 10.1107/s0108270100012816.

DOI:10.1107/s0108270100012816
PMID:11118980
Abstract

The hydrolysis product [Ga(2)(C(3)H(7))(4)(OH)(2)].C(14)H(32)N(4), derived from the tetrakis(triisopropylgallium)-1,4,8, 11-tetramethyl-1,4,8,11-tetraazacyclotetradecane (1/1) adduct, consists of a centrosymmetric (i)Pr(2)Ga(&mgr;-OH) unit hydrogen bonded through the hydroxyl group to a nitrogen on an adjacent centrosymmetric 1,4,8,11-tetramethyl-1,4,8, 11-tetraazacyclotetradecane molecule, resulting in the generation of a molecular chain through the crystal.

摘要

由四（三异丙基镓）-1,4,8,11-四甲基-1,4,8,11-四氮杂环十四烷（1/1）加合物衍生的水解产物[Ga(2)(C(3)H(7))(4)(OH)(2)].C(14)H(32)N(4)，由一个中心对称的(i)Pr(2)Ga(μ-OH)单元组成，该单元通过羟基与相邻中心对称的1,4,8,11-四甲基-1,4,8,11-四氮杂环十四烷分子上的一个氮形成氢键，从而在晶体中产生分子链。

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