Frankenberger R, Krämer N, Sindel J
Policlinic for Operative Dentistry and Periodontology, University of Erlangen-Nuremberg, Erlangen, Germany.
Oper Dent. 2000 May-Jun;25(3):209-15.
The purpose of this in vitro study was to examine shear bond strengths of composite resin to metal-exposed porcelain-fused-to-metal (PFM) and all-ceramic restorations after silica coating or etching with 5% hydrofluoric acid (HF). Specimens were fabricated for each of the following groups: two all-ceramic materials [a feldspathic porcelain (Vita Mark II) and a leucite-reinforced glass-ceramic (IPS Empress)], and one noble metal-ceramic (Orplid Keramik I alloy; Vita VMK 68 N felspathic veneer ceramic). These groups were repaired with resin composites after different pretreatment methods. In one metal-ceramic subgroup the surface exhibited a 50% metal and 50% ceramic exposure. In the silica-coating groups, the specimen surfaces were air abraded with silica acid-modified Al2O3 (CoJet Sand) and treated corresponding to the porcelain repair with resin composite. For control groups, the surfaces were etched with 5% HF for 60 seconds and treated in the same way as the silica-coated groups. After 24 hours of storage (distilled water, 37 degrees C) and an additional 24 hours of thermocycling (1150 x 5 degrees C/55 degrees C) the specimens were debonded using a shear bond strength test (n = 15). In all groups the silica coat repair achieved equal or significantly higher bond strengths than did the etching technique (p < 0.05, Mann-Whitney U test). In the metal-exposed group, the mean bond strength increased from 7.3 MPa to 16.3 MPa following the silica-coat repair. Results indicated that silica coating represents a suitable treatment for the intraoral repair of the materials tested in the present study.
本体外研究的目的是检测在进行二氧化硅涂层处理或用5%氢氟酸(HF)蚀刻后,复合树脂与金属暴露的烤瓷熔附金属(PFM)及全瓷修复体之间的剪切粘结强度。针对以下各组制作标本:两种全瓷材料[一种长石质瓷(维他马克Ⅱ)和一种白榴石增强玻璃陶瓷(IPS铸瓷)],以及一种贵金属陶瓷(奥普利德烤瓷合金Ⅰ;维他VMK 68 N长石质贴面陶瓷)。这些组在经过不同的预处理方法后用树脂复合材料进行修复。在一个金属陶瓷亚组中,表面呈现50%金属和50%陶瓷暴露。在二氧化硅涂层组中,标本表面用硅酸改性的Al2O3(CoJet Sand)进行空气喷砂处理,并按照用树脂复合材料修复瓷体的方法进行处理。对于对照组,表面用5% HF蚀刻60秒,并以与二氧化硅涂层组相同的方式进行处理。在储存24小时(蒸馏水,37℃)并额外进行24小时热循环(1150×5℃/55℃)后,使用剪切粘结强度测试使标本脱粘(n = 15)。在所有组中,二氧化硅涂层修复所获得的粘结强度等于或显著高于蚀刻技术(p < 0.05,曼-惠特尼U检验)。在金属暴露组中,二氧化硅涂层修复后平均粘结强度从7.3 MPa增加到16.3 MPa。结果表明,二氧化硅涂层是本研究中所测试材料口腔内修复的一种合适处理方法。