Department of Preventive Dentistry, Faculty of Dentistry, Jordan University of Science and Technology, Irbid, Jordan.
Eur J Orthod. 2010 Jun;32(3):274-80. doi: 10.1093/ejo/cjp098. Epub 2009 Nov 10.
The aims of this study were to evaluate the shear bond strength (SBS) of metal and ceramic brackets bonded to two different all-ceramic crowns, IPS Empress 2 and In-Ceram Alumina, to compare the SBS between hydrofluoric acid (HFA), phosphoric acid etched, and sandblasted, non-etched all-ceramic surfaces. Ninety-six all-ceramic crowns were fabricated resembling a maxillary left first premolar. The crowns were divided into eight groups: (1) metal brackets bonded to sandblasted 9.6 per cent HFA-etched IPS Empress 2 crowns; (2) metal brackets bonded to sandblasted 9.6 per cent HFA-etched In-Ceram crowns; (3) ceramic brackets bonded to sandblasted 9.6 per cent HFA-etched IPS Empress 2 crowns; (4) ceramic brackets bonded to sandblasted 9.6 per cent HFA-etched In-Ceram crowns; (5) metal brackets bonded to sandblasted 37 per cent phosphoric acid-etched IPS Empress 2 crowns; (6) metal brackets bonded to sandblasted 37 per cent phosphoric acid-etched In-Ceram crowns; (7) metal brackets bonded to sandblasted, non-etched IPS Empress 2 crowns; and (8) metal brackets bonded to sandblasted, non-etched In-Ceram crowns. Metal and ceramic orthodontic brackets were bonded using a conventional light polymerizing adhesive resin. An Instron universal testing machine was used to determine the SBS at a crosshead speed of 0.1 mm/minute. Comparison between groups was performed using a univariate general linear model and chi-squared tests. The highest mean SBS was found in group 3 (120.15 +/- 45.05 N) and the lowest in group 8 (57.86 +/- 26.20 N). Of all the variables studied, surface treatment was the only factor that significantly affected SBS (P < 0.001). Acid etch application to sandblasted surfaces significantly increased the SBS in groups 1, 2, 5, and 6. The SBS of metal brackets debonded from groups 1, 3, and 5 were not significantly different from those of groups 2, 4, and 6. All debonded metal brackets revealed a similar pattern of bond failure at the adhesive-restorative interface. However, ceramic brackets had a significantly different adhesive failure pattern with dominant failure at the adhesive-bracket interface. Ceramic fractures after bracket removal were found more often in groups 1-4. No significant difference in ceramic fracture was observed between the IPS Empress 2 and In-Ceram groups.
本研究的目的是评估金属和陶瓷托槽与两种不同全瓷冠(IPS Empress 2 和 In-Ceram Alumina)粘结后的剪切粘结强度(SBS),并比较氢氟酸(HFA)、磷酸酸蚀、喷砂和非酸蚀全瓷表面的 SBS。制备了 96 个类似于上颌左侧第一前磨牙的全瓷冠。将这些冠分为 8 组:(1)金属托槽粘结在喷砂 9.6%HFA 酸蚀 IPS Empress 2 冠上;(2)金属托槽粘结在喷砂 9.6%HFA 酸蚀 In-Ceram 冠上;(3)陶瓷托槽粘结在喷砂 9.6%HFA 酸蚀 IPS Empress 2 冠上;(4)陶瓷托槽粘结在喷砂 9.6%HFA 酸蚀 In-Ceram 冠上;(5)金属托槽粘结在喷砂 37%磷酸酸蚀 IPS Empress 2 冠上;(6)金属托槽粘结在喷砂 37%磷酸酸蚀 In-Ceram 冠上;(7)金属托槽粘结在喷砂、非酸蚀 IPS Empress 2 冠上;(8)金属托槽粘结在喷砂、非酸蚀 In-Ceram 冠上。金属和陶瓷正畸托槽使用常规光聚合胶粘剂粘结。使用 Instron 万能试验机以 0.1mm/min 的十字头速度测定 SBS。采用单变量一般线性模型和卡方检验对组间进行比较。第 3 组的平均 SBS 最高(120.15±45.05N),第 8 组最低(57.86±26.20N)。在所研究的所有变量中,表面处理是唯一显著影响 SBS 的因素(P<0.001)。酸蚀应用于喷砂表面显著增加了第 1、2、5 和 6 组的 SBS。第 1、3 和 5 组脱粘的金属托槽的 SBS 与第 2、4 和 6 组的 SBS 无显著差异。所有脱粘的金属托槽在粘结-修复界面处呈现相似的粘结破坏模式。然而,陶瓷托槽的粘结破坏模式明显不同,主要发生在粘结-托槽界面处。去除托槽后发现更多的陶瓷断裂发生在第 1-4 组。IPS Empress 2 组和 In-Ceram 组之间的陶瓷断裂无显著差异。