Yang W, Yang N, Wang T
Analysis and Testing Centre Ningxia University, Yinchuan, 750021.
Zhongguo Zhong Yao Za Zhi. 1997 Dec;22(12):732-4, 764.
Matrine and oxymatrine in Jieeryin and Fuyanshuan were separated and determined by Reversed Phase High Performance Liquid Chromatography, A chromatographic method for the separation and determination of matrine and oxymatrine in these preparations was established. Chromatographic coditions: ODS column with methanol-water-triethylamine(55:45:0.02) as the mobil phase, and UV detection at 215 nm. The method is simple, sensitive and accurate. This study provides the scientific basis for quality evaluation and quality control in making these preparations.
采用反相高效液相色谱法对洁尔阴和妇炎栓中的苦参碱和氧化苦参碱进行分离测定，建立了这两种制剂中苦参碱和氧化苦参碱的分离测定色谱方法。色谱条件：以甲醇 - 水 - 三乙胺（55∶45∶0.02）为流动相的ODS柱，在215 nm波长处进行紫外检测。该方法简便、灵敏、准确。本研究为这些制剂的质量评价和质量控制提供了科学依据。
