高效液相色谱法测定加味逍遥丸中栀子苷和芍药苷的含量
[Determination of geniposide and paeoniflorin in Jiawei Xiaoyao Pills by HPLC].
作者信息
Di L, Guo R, Xie H, Fan B
机构信息
Nanjing University of TCM, Nanjing 210029.
出版信息
Zhongguo Zhong Yao Za Zhi. 1997 Nov;22(11):671-3, 703.
PMID:11243183
Abstract
The geniposide and paeoniflorin in Jiaowei Xiaoyao Pills were separated and determined by HPLC, with a C18 column and a mixture of CH3CN-0.1% H3PO4(13:87) as mobile phase. The method is simple, rapid and accurate. The components have a good linearity, and the average recovery with RSD(n = 5) is 101.81% + 2.38% for geniposide and 98.75% + 1.95% for paeoniflorin.
摘要
采用高效液相色谱法（HPLC）对加味逍遥丸中的栀子苷和芍药苷进行分离测定，以C18柱，乙腈-0.1%磷酸（13:87）混合溶液为流动相。该方法简便、快速、准确。各成分线性关系良好，栀子苷平均回收率（n = 5）为101.81% ± 2.38%，芍药苷平均回收率为98.75% ± 1.95%。
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