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用于测定苹果中多酚的加压液体萃取法。

Pressurized liquid extraction for the determination of polyphenols in apple.

作者信息

Alonso-Salces R M, Korta E, Barranco A, Berrueta L A, Gallo B, Vicente F

机构信息

Department of Analytical Chemistry, Faculty of Sciences. Universidad del País Vasco/Euskal Herriko Unibertsitatea, P.O. Box 644. E-48080 Bilbao, Spain.

出版信息

J Chromatogr A. 2001 Nov 9;933(1-2):37-43. doi: 10.1016/s0021-9673(01)01212-2.

DOI:10.1016/s0021-9673(01)01212-2
PMID:11758745
Abstract

Pressurized liquid extraction (PLE) has been optimized for the determination of polyphenols in Golden Delicious apple peel and pulp. The effects of experimental variables, such as solvent composition, temperature, static extraction time and pressure, on PLE efficiency have been studied. Once the optimum conditions were established the recovery and the precision of the method for each analyte was tested by means of repeated analysis.

摘要

加压液体萃取（PLE）已针对金冠苹果果皮和果肉中多酚的测定进行了优化。研究了溶剂组成、温度、静态萃取时间和压力等实验变量对PLE效率的影响。确定最佳条件后，通过重复分析对每种分析物方法的回收率和精密度进行了测试。

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