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Fluorinated protective groups for on-resin quantification of solid-phase oligosaccharide synthesis with 19F NMR spectroscopy.

作者信息

Mogemark Mickael, Elofsson Mikael, Kihlberg Jan

机构信息

Organic Chemistry, Department of Chemistry, Umeå University, 90187 Umeå, Sweden.

出版信息

Chembiochem. 2002 Dec 2;3(12):1266-9. doi: 10.1002/1439-7633(20021202)3:12<1266::AID-CBIC1266>3.0.CO;2-6.

DOI:10.1002/1439-7633(20021202)3:12<1266::AID-CBIC1266>3.0.CO;2-6

PMID:12465038

Abstract

摘要

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Synthesis and application of a 2-[(4-fluorophenyl)-sulfonyl]ethoxy carbonyl(Fsec) protected glycosyl donor in carbohydrate chemistry.

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相似文献

Fluorinated protective groups for on-resin quantification of solid-phase oligosaccharide synthesis with 19F NMR spectroscopy.

Chembiochem. 2002 Dec 2;3(12):1266-9. doi: 10.1002/1439-7633(20021202)3:12<1266::AID-CBIC1266>3.0.CO;2-6.

Gel-phase 19F NMR spectral quality for resins commonly used in solid-phase organic synthesis; a study of peptide solid-phase glycosylations.

Org Biomol Chem. 2004 Jun 21;2(12):1770-6. doi: 10.1039/b404802d. Epub 2004 May 25.

Solid-phase synthesis of alpha-Gal epitopes: on-resin analysis of solid-phase oligosaccharide synthesis with 19F NMR spectroscopy.

J Org Chem. 2003 Sep 19;68(19):7281-8. doi: 10.1021/jo034581x.

NMR tube filter reactor for solid-phase synthesis and gel-phase 19F NMR spectroscopy.

J Comb Chem. 2006 Mar-Apr;8(2):150-2. doi: 10.1021/cc050144f.

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Chem Asian J. 2006 Dec 18;1(6):798-813. doi: 10.1002/asia.200600210.

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引用本文的文献

Synthesis and application of a 2-[(4-fluorophenyl)-sulfonyl]ethoxy carbonyl(Fsec) protected glycosyl donor in carbohydrate chemistry.

Molecules. 2010 Aug 19;15(8):5708-20. doi: 10.3390/molecules15085708.

Fluorinated protective groups for on-resin quantification of solid-phase oligosaccharide synthesis with 19F NMR spectroscopy.

作者信息

Mogemark Mickael, Elofsson Mikael, Kihlberg Jan

机构信息

Organic Chemistry, Department of Chemistry, Umeå University, 90187 Umeå, Sweden.

出版信息

Chembiochem. 2002 Dec 2;3(12):1266-9. doi: 10.1002/1439-7633(20021202)3:12<1266::AID-CBIC1266>3.0.CO;2-6.

DOI:10.1002/1439-7633(20021202)3:12<1266::AID-CBIC1266>3.0.CO;2-6

PMID:12465038

Abstract

摘要