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大麻素及其单加氧衍生物的色谱分离

Chromatographic separation of cannabinoids and their monooxygenated derivatives.

作者信息

Fonseka K, Widman M

出版信息

J Chromatogr. 1976 May 26;120(2):334-8.

PMID:1270554
Abstract

delta1-Tetrahydrocannabinol, delta6-tetrahydrocannabinol, cannabinol, cannabidiol and several of their monooxygenated derivatives have been separated from each other by a combination of liquid, thin-layer and gas chromatography. Retention volumes (on Sephadex LH-20), Rf values and retention times can be recorded, and may provide guidance in the separation and identification of these known cannabinoids.

摘要

通过液相色谱、薄层色谱和气相色谱联用的方法,已将δ1-四氢大麻酚、δ6-四氢大麻酚、大麻酚、大麻二酚及其几种单加氧衍生物彼此分离。可以记录(在葡聚糖凝胶LH-20上的)保留体积、比移值和保留时间,这些数据可为分离和鉴定这些已知大麻素提供指导。

相似文献

1
Chromatographic separation of cannabinoids and their monooxygenated derivatives.大麻素及其单加氧衍生物的色谱分离
J Chromatogr. 1976 May 26;120(2):334-8.
2
Characterization of the butyl homologues of delta1-tetrahydrocannabinol, cannabinol and cannabidiol in samples of cannabis by combined gas chromatography and mass spectrometry.采用气相色谱-质谱联用技术对大麻样品中δ1-四氢大麻酚、大麻酚和大麻二酚的丁基同系物进行表征。
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[Cannabis plants cultivated in Germany: substances in the sense of the narcotics law?].
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The separation, identification, and quantitation of cannabinoids and their tau=butyldimethylsilyl, trimethylsilylacetate, and diethylphosphate derivatives using high-pressure liquid chromatography, gas-liquid chromatography, and mass spectrometry.使用高压液相色谱法、气液色谱法和质谱法对大麻素及其叔丁基二甲基硅烷基、三甲基硅烷基乙酸酯和二乙基磷酸酯衍生物进行分离、鉴定和定量。
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Synthesis and characterization of glucuronides of Cannabinol, cannabidiol, delta9-tetrahydrocannabinol and delta8-tetrahydrocannabinol.大麻酚、大麻二酚、Δ9-四氢大麻酚和Δ8-四氢大麻酚葡糖醛酸苷的合成与表征
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Diazotized dapsone as a reagent for the detection of cannabinoids on thin-layer chromatographic plates.重氮化氨苯砜作为在薄层色谱板上检测大麻素的试剂。
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