大麻酚、大麻二酚、Δ9-四氢大麻酚和Δ8-四氢大麻酚葡糖醛酸苷的合成与表征
Synthesis and characterization of glucuronides of Cannabinol, cannabidiol, delta9-tetrahydrocannabinol and delta8-tetrahydrocannabinol.
作者信息
Lyle M A, Pallante S, Head K, Fenselau C
出版信息
Biomed Mass Spectrom. 1977 Jun;4(3):190-6. doi: 10.1002/bms.1200040313.
PMID:890081
Abstract
Partially purified glucuronyltransferase immobilized on beaded sepharose has been used to synthesize the glucuronide conjugates of cannabinol, cannabidol, delta9-tetrahydrocannabinol and delta8-tetrahydrocannabinol. Trimethylsilylated methyl esters and per(trimethylsilyl) derivatives of these conjugates have been characterized by their gas chromatographic retention times and their electron impact and ammonia chemical ionization mass spectra.
摘要
固定在琼脂糖珠上的部分纯化的葡糖醛酸基转移酶已被用于合成大麻酚、大麻二酚、δ9-四氢大麻酚和δ8-四氢大麻酚的葡糖醛酸缀合物。这些缀合物的三甲基硅烷基化甲酯和全（三甲基硅烷基）衍生物已通过其气相色谱保留时间以及电子轰击和氨化学电离质谱进行了表征。
Zotero 插件