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采用气相色谱-质谱联用技术对大麻样品中δ1-四氢大麻酚、大麻酚和大麻二酚的丁基同系物进行表征。

Characterization of the butyl homologues of delta1-tetrahydrocannabinol, cannabinol and cannabidiol in samples of cannabis by combined gas chromatography and mass spectrometry.

作者信息

Harvey D J

出版信息

J Pharm Pharmacol. 1976 Apr;28(4):280-5. doi: 10.1111/j.2042-7158.1976.tb04153.x.

DOI:10.1111/j.2042-7158.1976.tb04153.x
PMID:6715
Abstract

The butyl homologues of delta1-tetrahydrocannabinol, delta1-tetrahydrocannabinolic acid, cannabinol and cannabidiol have been identified in several samples of cannabis. 8 samples contained delta1-tetrahydrocannabinolic acid, one sample contained cannabinol and one sample contained both cannabinol and cannabidiol. Separation by gas chromatography and identification by gas chromotography-mass spectrometry was achieved by the preparation of trimethylsilyl, d9-trimethylsilyl, triethylsilyl and tri-n-propylsilyl derivatives.

摘要

在大麻的多个样本中已鉴定出δ1-四氢大麻酚、δ1-四氢大麻酚酸、大麻酚和大麻二酚的丁基同系物。8个样本含有δ1-四氢大麻酚酸，1个样本含有大麻酚，1个样本同时含有大麻酚和大麻二酚。通过制备三甲基硅烷基、d9-三甲基硅烷基、三乙基硅烷基和三正丙基硅烷基衍生物，实现了气相色谱分离和气相色谱-质谱鉴定。

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Characterization of the butyl homologues of delta1-tetrahydrocannabinol, cannabinol and cannabidiol in samples of cannabis by combined gas chromatography and mass spectrometry.采用气相色谱-质谱联用技术对大麻样品中δ1-四氢大麻酚、大麻酚和大麻二酚的丁基同系物进行表征。
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