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血浆3-羟基-17-氧代甾体硫酸盐的提取及成分硫酸脱氢表雄酮和硫酸雄酮的测定。

THE EXTRACTION OF PLASMA 3-HYDROXY-17-OXO STEROID SULPHATES AND THE MEASUREMENT OF THE CONSTITUENT DEHYDROEPIANDROSTERONE SULPHATE AND ANDROSTERONE SULPHATE.

作者信息

MCKENNA J, RIPPON A E

出版信息

Biochem J. 1965 Apr;95(1):107-17. doi: 10.1042/bj0950107.

DOI:10.1042/bj0950107
PMID:14333546
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC1215184/
Abstract
  1. A simple method for the extraction of 17-oxo steroid sulphates of plasma is described; glucosiduronates and orthophosphates are extracted, but to a smaller extent. 2. Four methods of analyses of the extracts are given and are relatively simple. Three of these are specific for steroid sulphates and two measure the sulphate conjugates directly. 3. Values for dehydroepiandrosterone sulphate and androsterone sulphate concentrations of normal and pathological plasmas are given.
摘要
  1. 本文描述了一种从血浆中提取17-氧代甾体硫酸盐的简单方法；葡萄糖醛酸苷和正磷酸盐也能被提取，但程度较小。2. 给出了四种提取物的分析方法，这些方法相对简单。其中三种对甾体硫酸盐具有特异性，两种可直接测定硫酸盐结合物。3. 给出了正常和病理血浆中硫酸脱氢表雄酮和硫酸雄酮浓度的值。

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Acta Soc Med Ups. 1964;69:105-24.

引用本文的文献

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The indirect analysis of 17-oxosteroid glucosiduronates and sulphates in human urine.人尿中17-氧代类固醇葡糖苷酸酯和硫酸盐的间接分析。
Biochem J. 1966 Jun;99(3):747-59. doi: 10.1042/bj0990747.
2
16Beta-hydroxylation of dehydroepiandrosterone sulphate by homogenates of human foetal liver.硫酸脱氢表雄酮在人胎儿肝脏匀浆中的16β-羟基化作用
Biochem J. 1976 May 15;156(2):419-25. doi: 10.1042/bj1560419.

本文引用的文献

1
The oxidation of steroids with tert.-butyl chromate.用叔丁基铬酸酯氧化甾体化合物。
Biochem J. 1962 Jul;84(1):195-201. doi: 10.1042/bj0840195.
2
Methods of paper chromatography of steroids applicable to the study of steroids in mammalian blood and tissues.适用于研究哺乳动物血液和组织中类固醇的类固醇纸色谱法。
Biochem J. 1952 Jan;50(3):370-8. doi: 10.1042/bj0500370.
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Determination of dehydroepian-drosterone, androsterone, etiocholanolone, and "11 beta-hydroxyetiocholanolone" in plasma.
Clin Chim Acta. 1962 Mar;7:221-5. doi: 10.1016/0009-8981(62)90013-x.
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Isolation of dehydroepiandrosterone and 17alpha-hydroxy-delta5-pregenolone from the polycystic ovaries of the Stein-Leventhal syndrome.从斯坦因-莱文塔尔综合征的多囊卵巢中分离脱氢表雄酮和17α-羟基-δ5-孕烯醇酮。
J Clin Endocrinol Metab. 1962 Apr;22:441-8. doi: 10.1210/jcem-22-4-441.
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Some aspects of the Zimmermann reaction.齐默尔曼反应的某些方面。
Biochem J. 1962 Jun;83(3):583-8. doi: 10.1042/bj0830583.
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Studies of conjugated 17-ketosteroids in a case of adrenal tumor.肾上腺肿瘤病例中结合17-酮类固醇的研究。
J Clin Endocrinol Metab. 1962 May;22:501-10. doi: 10.1210/jcem-22-5-501.
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[Quantitative and qualitative determination of steroid sulfates with the aid of methylene blue. II. Detection of steroid sulfates by paper chromatography].[借助亚甲蓝对甾体硫酸盐进行定量和定性测定。II. 用纸色谱法检测甾体硫酸盐]
Rev Fr Etud Clin Biol. 1960 Mar;5:284-6.
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Three sulfate esters of 17-ketosteroids in the plasma of normal subjects and after administration of ACTH.正常受试者血浆中及注射促肾上腺皮质激素后的17-酮类固醇的三种硫酸酯。
J Clin Endocrinol Metab. 1960 Jun;20:900-4. doi: 10.1210/jcem-20-6-900.
9
Isolation and identification of etiocholan-3 alpha-ol-17-one and etiocholane-3 alpha, 11 beta-diol-17-one from human blood plasma.
Arch Biochem Biophys. 1961 Jan;92:150-3. doi: 10.1016/0003-9861(61)90229-6.
10
Quantitative paper chromatography of conjugated 17-ketosteroids in plasma.血浆中结合17-酮类固醇的定量纸色谱法。
J Clin Invest. 1961 Jun;40(6):947-53. doi: 10.1172/JCI104334.