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Thermal desorption-gas chromatography for the determination of benzene, aniline, nitrobenzene and chlorobenzene in workplace air.

作者信息

Patil S F, Lonkar S T

机构信息

Department of Chemistry and School of Environmental Sciences, University of Poona, India.

出版信息

J Chromatogr. 1992 May 29;600(2):344-51. doi: 10.1016/0021-9673(92)85571-a.

DOI:10.1016/0021-9673(92)85571-a
PMID:1492873
Abstract

Sampling on Tenax TA of different mesh sizes followed by thermal desorption and gas chromatography was evaluated as a simple method for the determination of benzene, aniline, nitrobenzene and chlorobenzene in the workplace air. An alternative sampling technique in place of pump sampling was developed. Quantitative recoveries were obtained in the mass range 0.04-10 micrograms. It was found that air humidity had no effect on recovery. The charged tubes can be stored at room temperature for 5 days with no change in recovery. The particle size of Tenax TA has no significant effect on adsorption and desorption.

摘要

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