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用于原子发射光谱分析的微波等离子体腔组件。

A microwave plasma cavity assembly for atomic emission spectrometry.

作者信息

Matusiewicz H

机构信息

Department of Analytical Chemistry, Politechnika Poznańska, 60-965, Poznań, Poland.

出版信息

Anal Bioanal Chem. 1996 Jun;355(5-6):623-5. doi: 10.1007/s0021663550623.

DOI:10.1007/s0021663550623
PMID:15045327
Abstract

Although inductively coupled plasmas (ICPs) are widely used for multielement analysis microwave induced plasma (MIP) offers a great potential for a variety of applications. Modifications to incorporate MIP into commercial ICP direct reading spectrometer systems have been developed. A direct reading échelle spectrometer is described which opens new possibilities for the successful construction of commercial MIP-AES systems with the potential to run all of the typical methods worked out for earlier ICP-AES applications. Use of flow injection techniques and automation to couple with in situ concentration will likely offer a further improvement in the analytical performance of this system. Due to the capabilities demonstrated by this spectrometer it appears that hybrid instruments will be increasingly important for future developments in optical spectrometry. This is particularly true for very demanding areas such as atomic emission spectrometry. The system could be readily commercialized.

摘要

虽然电感耦合等离子体(ICP)广泛用于多元素分析,但微波诱导等离子体(MIP)在各种应用中具有巨大潜力。已开发出将MIP纳入商用ICP直读光谱仪系统的改进方法。本文描述了一种直读阶梯光栅光谱仪,它为成功构建商用MIP-AES系统开辟了新的可能性,该系统有潜力运行所有为早期ICP-AES应用制定的典型方法。使用流动注射技术和自动化技术与原位富集相结合,可能会进一步提高该系统的分析性能。由于该光谱仪所展示的能力,混合仪器对于光谱学未来的发展似乎将变得越来越重要。在诸如原子发射光谱法等要求非常高的领域尤其如此。该系统可以很容易地实现商业化。

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