Nguyen N C, Maloney W J, Dauskardt R H
Department of Materials Science and Engineering, Stanford University, CA 94305-2205, USA.
J Mater Sci Mater Med. 1997 Aug;8(8):473-83. doi: 10.1023/a:1018574109544.
Fracture mechanics tests were performed to characterize the fracture toughness and fatigue crack-growth behaviour of polymethylmethacrylate (PMMA) bone cement, commonly used in joint replacement surgery. Compact tension specimens of various thicknesses were prepared and tested in both air and Ringer's solution. Contrary to previous reports citing toughness as a single valued parameter, the PMMA was found to exhibit resistance-curve behaviour with a plateau toughness of approximately 0.6 MPa m1/2 in air, and approximately 2.0 MPa m1/2 in Ringer's solution. The increased toughness in Ringer's solution is thought to arise from the plasticizing effect of the environment. Under cyclic loads, the material displayed true mechanical fatigue failure in both environments; fatigue crack-growth rates, da/dN, were measured over the range approximately 10(-10) to 10(-6) m/cycle and found to display a power-law dependence on the stress intensity range, DeltaK. The cement was found to be more resistant to fatigue-crack propagation in Ringer's solution than in air. Wear debris was observed on the fatigue fracture surfaces, particularly those produced in air. These findings and the validity of using a linear-elastic fracture mechanics approach for viscoelastic materials are discussed in the context of providing more reliable and fracture-resistant cemented joints.
进行了断裂力学试验,以表征常用于关节置换手术的聚甲基丙烯酸甲酯(PMMA)骨水泥的断裂韧性和疲劳裂纹扩展行为。制备了各种厚度的紧凑拉伸试样,并在空气和林格氏液中进行测试。与之前将韧性作为单一值参数的报道相反,发现PMMA呈现阻力曲线行为,在空气中的平台韧性约为0.6MPa·m1/2,在林格氏液中约为2.0MPa·m1/2。林格氏液中韧性的增加被认为是环境的增塑作用所致。在循环载荷下,该材料在两种环境中均表现出真正的机械疲劳失效;在约10(-10)至10(-6)m/循环的范围内测量了疲劳裂纹扩展速率da/dN,发现其对应力强度范围ΔK呈现幂律依赖性。发现该骨水泥在林格氏液中比在空气中更能抵抗疲劳裂纹扩展。在疲劳断口表面观察到磨损碎屑,尤其是在空气中产生的断口表面。在提供更可靠和抗断裂的骨水泥关节的背景下,讨论了这些发现以及对粘弹性材料使用线弹性断裂力学方法的有效性。