Loguercio Alessandro D, Uceda-Gomez Ninoshka, Carrilho Marcela Rocha de Oliveira, Reis Alessandra
School of Dentistry, University of Oeste de Santa Catarina, Joaçaba, SC, Brazil.
Dent Mater. 2005 Mar;21(3):224-31. doi: 10.1016/j.dental.2004.03.012.
Verify whether the dimension of a bonded specimen stored prior microtensile testing and its regional variation may affect the resin-dentin bond strength (BS) over time.
Thirty human third molars had a flat dentin surface exposed and all peripheral enamel removed. Two adhesive systems (Single-Bond and One-Step) were applied and composite resin crowns (Z250) were constructed. Teeth were divided into three groups (n = 5). Group A specimens were sectioned to obtain sticks to be tested in tension (0.5 mm/min) immediately. Group B specimens were stored in water for 6 months, before sectioning and testing. Group C specimens were sectioned; the sticks were stored for 6 months and tested. In groups A and B, the origin of the sticks, periphery and inner regions was controlled. Bond strength (BS) was expressed as an index that considers cohesive failures and estimated values of premature debonded specimens. One-way ANOVA and Tukey's test (alpha = 0.05) were used to compare groups A, B and C, and a second analytical approach (A and B) employed a two-way ANOVA (time versus regional differences) for each adhesive system.
For Single-Bond (SB), the BS for specimens in group A was higher than for groups B and C. For One-Step (OS), the BS in group A was higher than for B, which was in turn higher than for C. In the second group approach, no difference was found when the test was performed immediately; however, after 6 months, the inner sticks from group B showed significantly higher BS.
(1) The amount of decrease in BS is dependent on the specimen size; (2) the decrease in BS was greater for peripheral specimens than more centrally located specimens.
验证在进行微拉伸测试之前储存的粘结样本的尺寸及其区域差异是否会随时间影响树脂-牙本质粘结强度(BS)。
30颗人类第三磨牙暴露平坦的牙本质表面,并去除所有周边釉质。应用两种粘结系统(Single-Bond和One-Step)并构建复合树脂冠(Z250)。牙齿分为三组(n = 5)。A组样本立即切片以获得用于拉伸测试(0.5 mm/分钟)的棒材。B组样本在切片和测试前在水中储存6个月。C组样本切片;棒材储存6个月后进行测试。在A组和B组中,控制棒材的来源、周边和内部区域。粘结强度(BS)表示为一个考虑内聚破坏和过早脱粘样本估计值的指标。使用单向方差分析和Tukey检验(α = 0.05)比较A组至C组,第二种分析方法(A组和B组)对每种粘结系统采用双向方差分析(时间与区域差异)。
对于Single-Bond(SB),A组样本的BS高于B组和C组。对于One-Step(OS),A组的BS高于B组,B组又高于C组。在第二种分组方法中,立即进行测试时未发现差异;然而,6个月后,B组的内部棒材显示出明显更高的BS。
(1)BS降低的量取决于样本大小;(2)周边样本的BS降低比位于更中心位置的样本更大。